Textile auxiliary agent for auxiliary textile sizing and preparation method thereof

A textile auxiliaries and textile technology, applied in the field of textile auxiliaries for assisting textile sizing and its preparation, can solve the problems of little help in sizing effects, insignificant effects, and large dosage required

Inactive Publication Date: 2016-07-06
WUJIANG FUHUIYUAN HOME TEXTILES CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003]However, conventional textile auxiliaries often do little to help the sizing effect of fabrics

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0009] The preparation method of the textile auxiliaries of described auxiliary textile sizing comprises the following steps:

[0010] (1) Weigh each raw material according to parts by weight;

[0011] (2) Sodium dioctyl sulfosuccinate, ethyl formamidothiazole acetate, propyltriethoxysilane, 5-aminolevulinic acid, zinc phenolsulfonate, diphenyltridecyl phosphite , laurate, and polymethylsilicone resin, add 10% NaOH solution to adjust the pH to 8.5, and stir at 7500-8500r / m for 6-10h;

[0012] (3) Heat the stirred mixture to 65-75°C, then add azobisisobutyronitrile, nonylphenol polyoxyethylene ether, hydroxypropyl methylcellulose, and nano-graphite powder, and carry out the process in an ultrasonic machine. Ultrasound for the first time, then add cross-linking agent and softener, and perform the second ultrasonic to obtain the finished product.

[0013] Preferably, in the step (3), the first ultrasonic power is 800w, and the ultrasonic time is 6-7h, and the second ultrasonic ...

Embodiment 1

[0019] (1) Weigh 45 parts of dioctyl sodium sulfosuccinate, 40 parts of ethyl formylaminothiazole acetate, 35 parts of propyltriethoxysilane, 35 parts of 5-aminolevulinic acid, sulfonol Zinc acid 30 parts, diphenyltridecyl phosphite 25 parts, laurate 20 parts, polymethyl silicone resin 15 parts, azobisisobutyronitrile 15 parts, nonylphenol polyoxyethylene ether 10 parts, 5 parts of hydroxypropyl methylcellulose, 5 parts of nano graphite powder, 5 parts of polyisocyanate, 5 parts of silicone oil softener;

[0020] (2) Sodium dioctyl sulfosuccinate, ethyl formamidothiazole acetate, propyltriethoxysilane, 5-aminolevulinic acid, zinc phenolsulfonate, diphenyltridecyl phosphite , laurate, and polymethylsilicone resin, add 10% NaOH solution to adjust the pH to 8.5, and stir for 6 hours at 7500r / m;

[0021] (3) Heat the stirred mixture to 65°C, then add azobisisobutyronitrile, nonylphenol polyoxyethylene ether, hydroxypropyl methylcellulose, and nano-graphite powder, and perform the...

Embodiment 2

[0024] (1) Weigh 50 parts of dioctyl sodium sulfosuccinate, 45 parts of ethyl formylaminothiazole acetate, 40 parts of propyltriethoxysilane, 40 parts of 5-aminolevulinic acid, sulfonol Zinc acid 35 parts, diphenyltridecyl phosphite 30 parts, laurate 25 parts, polymethyl silicone resin 20 parts, azobisisobutyronitrile 20 parts, nonylphenol polyoxyethylene ether 15 parts, 10 parts of hydroxypropyl methylcellulose, 7 parts of nano graphite powder, 7 parts of polyether amino-modified polysiloxane, 7 parts of ester quaternary ammonium salt;

[0025] (2) Sodium dioctyl sulfosuccinate, ethyl formamidothiazole acetate, propyltriethoxysilane, 5-aminolevulinic acid, zinc phenolsulfonate, diphenyltridecyl phosphite , laurate, polymethyl silicone resin mixed, adding 10% NaOH solution to adjust the pH to 8.5, stirring at 8000r / m for 8h;

[0026] (3) Heat the stirred mixture to 70°C, then add azobisisobutyronitrile, nonylphenol polyoxyethylene ether, hydroxypropyl methylcellulose, and nan...

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PUM

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Abstract

The invention discloses a textile auxiliary agent for auxiliary textile sizing. The textile auxiliary agent is prepared from, by weight, 45-55 parts of sodium diethylhexyl sulfosuccinate, 40-50 parts of formamidothiazol-4-acetic acid ethyl ester, 35-45 parts of propyltriethoxysilane, 35-45 parts of 5-aminolevulinic acid, 30-40 parts of zinc phenolsulfonate, 25-35 parts of diphenyl tridecyl phosphite, 20-30 parts of laurate, 15-25 parts of methyl silicone resin, 15-25 parts of azodisisobutyronitrile, 10-20 parts of nonylphenol polyoxyethylene ether, 5-15 parts of hydroxypropyl methyl cellulose, 5-10 parts of nano-graphite powder, 5-10 parts of a cross-linking agent and 5-10 parts of a softening agent. Accordingly, the sizing efficiency can be improved, and the effect that size permeates into a fabric is enhanced. The invention further discloses a corresponding preparation method.

Description

technical field [0001] The invention relates to the technical field of textile auxiliaries, in particular to a textile auxiliaries for assisting textile sizing and a preparation method thereof. Background technique [0002] Textile auxiliaries are necessary chemicals in the process of textile production and processing. Textile auxiliaries play an indispensable role in improving the product quality and added value of textiles. It can not only endow textiles with various special functions and styles, such as softness, wrinkle resistance, shrink resistance, waterproof, antibacterial, antistatic, flame retardant Etc., can also improve the dyeing and finishing process, play a role in saving energy and reducing processing costs. Textile auxiliaries are crucial to improving the overall level of the textile industry and their role in the textile industry chain. Existing textile auxiliaries mainly include scouring agent, dyeing agent, leveling agent, softener, hair effect enhancer,...

Claims

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Application Information

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IPC IPC(8): D06M13/256D06M13/402D06M13/513D06M13/288D06M13/224D06M15/53D06M15/09D06M11/74D06M13/342
CPCD06M13/256D06M11/74D06M13/224D06M13/288D06M13/342D06M13/402D06M13/513D06M15/09D06M15/53
Inventor 沈飞峰
Owner WUJIANG FUHUIYUAN HOME TEXTILES CO LTD
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