A method for CO2 reduction by metal oxide modified electrode biofilm
An oxide and biofilm technology, applied in chemical instruments and methods, electrochemical biocombination treatment, separation methods, etc., to achieve the effects of low price, improved ability to obtain electrons, and improved electrochemical performance
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Embodiment 1
[0064] Step (1): Using a three-electrode system for CV scanning to prepare iron oxide modified conductive carbon cloth:
[0065] In a three-electrode system, Fe 2+ The precursor solution is used as the electrolyte, the conductive substrate is used as the working electrode, the titanium electrode is used as the counter electrode, and the Ag / AgCl electrode is used as the reference electrode; the specific steps are as follows:
[0066] Step (1-1): Take 200mL acetate buffer solution (the concentration of sodium acetate is 0.2mol / L) and configure 10mmol / L FeSO 4 solution, and adjust the pH of the solution to 7.0 with acetic acid to obtain Fe 2+ The precursor solution;
[0067] Step (1-2): the configured Fe 2+ The precursor solution was transferred to the beaker, the above-mentioned three-electrode system was installed, and connected to the electrochemical workstation.
[0068] Step (1-3): Set the CV scanning range of the workstation to 0.1-1.6V, the scanning speed to 50mV / s, an...
Embodiment 2
[0076] The difference from Example 1 is that in step (1), Cu 2+ The precursor solution was used to modify the conductive carbon cloth.
[0077] Cu 2+ The precursor solution is Cu(CH with a concentration of 10mmol / L 3 COO) 2 An acetate-buffered saline solution with a pH of 5.5.
[0078] The CV scanning range of the workstation is -1.0-0.4V, the scanning speed is 50mV / s, and the number of scanning circles is 50 circles.
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