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A recovery treatment agent for lauric acid modified magnetorheological fluid and its preparation method

A magnetorheological fluid, recycling technology, applied in magnetic fluids, water/sewage treatment, chemical instruments and methods, etc., to achieve the effect of increasing porosity, enhancing lipophilic and hydrophobicity, and simple components

Inactive Publication Date: 2019-01-11
MAANSHAN FULAIYI ENVIRONMENT PROTECTION TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] Aiming at the problems that the oleic acid-modified magnetorheological fluid cannot be recovered and treated in the prior art, and there is secondary pollution, the present invention provides a recovery treatment agent for the lauric acid-modified magnetorheological fluid and its preparation method, which can be processed by using The agent changes the properties of lauric acid in the magnetorheological fluid, improves its lipophilicity and hydrophobicity, and greatly weakens the interaction between the surfactant and the main dispersed particles, resulting in the interaction between the main dispersed particles and the carrier liquid in the magnetorheological fluid. The bonding effect is eliminated, so that the main dispersed particles can settle rapidly under the action of their own gravity, so that the main dispersed particles and the carrier liquid are separated, which provides a basis for the subsequent recycling of magnetorheological fluid

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] The magnetorheological fluid treated in this example is a magnetorheological fluid with lauric acid as the main component of the surfactant, the main dispersed particles are hydroxyl iron powder, the magnetic saturation is 2.1T, and the carrier fluid is mineral oil. The magnetorheological fluid waste to be treated is the solution after its use exceeds its shear fatigue life. At this time, the change of its zero-shear viscosity and adjustable multiple exceeds ±10% during the inspection process; The composition of the recovery treatment agent used in the embodiment and the mass parts of each component are: based on the total number of parts as 100 parts, 18 parts of corncobs, 18 parts of peanut shells, and 6 parts of sodium dodecylbenzenesulfonate , 3 parts of methanol, and the rest are deionized water. The specific preparation method is:

[0035] (1) crushing corncobs and peanut shells respectively, and sieving corncob powder and peanut shell powder with a particle size ...

Embodiment 2

[0047] The magnetorheological fluid treated in this example is a magnetorheological fluid with lauric acid as the main component of the surfactant, the main dispersed particles are hydroxyl iron powder, the magnetic saturation is 2.1T, and the carrier fluid is mineral oil. The magnetorheological fluid waste to be treated is the solution after its use exceeds its shear fatigue life. At this time, the change of its zero-shear viscosity and adjustable multiple exceeds ±10% during the inspection process; The composition of the recycling agent used in the embodiment and the mass parts of each component are: based on 100 parts of the total parts, 15 parts of corncobs, 20 parts of peanut shells, and 5 parts of sodium dodecylbenzenesulfonate , 2 parts of methanol, and the rest are deionized water. The specific preparation method is:

[0048] (1) crushing corncobs and peanut shells respectively, and sieving corncob powder and peanut shell powder with a particle size of 4 to 10 mm;

[...

Embodiment 3

[0060] The magnetorheological fluid treated in this example is a magnetorheological fluid with lauric acid as the main component of the surfactant, the main dispersed particles are pure iron powder, the magnetic saturation is 2.2T, and the carrier fluid is dimethyl silicone oil. The magnetorheological fluid waste to be treated in the embodiment is the solution after its use exceeds its shear fatigue life. At this time, the variation of its zero-shear viscosity and adjustable multiple exceeds ±10% during the inspection process The composition of the recycling treatment agent that the present embodiment adopts and the mass parts of each component are: take total parts as 100 parts, corncob is 20 parts, peanut shell 15 parts, sodium dodecylbenzene sulfonate 8 parts, 5 parts of methanol, and the rest are deionized water. The specific preparation method is:

[0061] (1) crushing corncobs and peanut shells respectively, and sieving corncob powder and peanut shell powder with a parti...

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Abstract

The invention discloses a recycling agent for a magnetorheological fluid modified by lauric acid and a preparation method for the recycling agent, and belongs to the technical field of recycling of the magnetorheological fluid. The recycling agent comprises the following components in parts by mass (based on 100 parts): 15-20 parts of corn cobs, 15-20 parts of peanut shells, 5-8 parts of sodium dodecyl benzene sulfonate and the balance of water. According to the recycling agent, hydroxyls contained on cellulose, hemicellulose and lignin of a biological material and carboxyl on lauric acid generate esterification reaction to form an alkyl chain in which an ester group is connected with lauric acid, so that the lipophilic-hydrophobic property is strengthened; due to the pore-forming effect of the recycling agent, micro pores of the biological material are further increased, and the porosity of the biological material is increased, therefore, main dispersion particles in the magnetorheological fluid settle; and moreover, due to the adsorption effect of the biological material, a surfactant and an additive are adsorbed, so that other components in the magnetorheological fluid are further separated, and the effect of treating waste with waste is achieved.

Description

technical field [0001] The invention belongs to the technical field of recovery and treatment of magnetic waste liquid, and more specifically relates to a recovery treatment agent for lauric acid-modified magnetorheological fluid and a preparation method thereof. Background technique [0002] Magnetorheological Fluid (MR fluid for short) is a controllable fluid, which is a relatively active research in smart materials. Magnetorheological fluid is a suspension formed by mixing tiny soft magnetic particles with high magnetic permeability and low magnetic hysteresis and non-magnetic liquid. Magnetorheological fluid has been widely valued for its unique magnetorheological effect. Magnetorheological fluid is a suspension formed by distributing micron-scale ferromagnetic particles in a non-magnetic liquid. Under the action of an external magnetic field, the properties of the magnetorheological fluid (such as rheology, magnetism, mechanics, heat, optics, etc.) change rapidly, fro...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C02F9/04C02F9/12H01F1/44
CPCC02F1/286C02F1/488C02F1/5263C02F9/00C02F2305/04H01F1/447
Inventor 邢战伟胡聪刘鹏
Owner MAANSHAN FULAIYI ENVIRONMENT PROTECTION TECH CO LTD
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