Novel ceramic ink-jet ink and production process thereof
A ceramic inkjet and ink technology, which is applied in the field of architectural ceramic decoration, can solve the problems of particle agglomeration and low stability, unstable surface tension of ink, and low solubility of ceramic powder, etc. Color and stable effect
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Embodiment 1
[0043] Embodiment 1-a kind of production technology of ceramic ink-jet ink, comprises the steps:
[0044] (1) Weigh 38% of the soluble metal salt and 60% of the water-soluble organic solvent to dissolve it, put it into the reaction kettle for heating reaction, and filter the residue after cooling;
[0045] Wherein: the soluble metal salt is a combination of copper sulfate, copper acetate and copper nitrate; the water-soluble organic solvent is ethanol, accounting for 29% of the ink solution; the auxiliary material accounts for 1% of the ink solution.
[0046] (2) Add dispersant to the reaction kettle in step (1), and add 0.05% pH regulator to adjust the pH value to 7;
[0047] (3) Put the remaining 40% water-soluble organic solvents and additives into the reaction solution for reaction;
[0048] (4) After completely dissolving and reacting, cool, filter with 350 mesh and 800 mesh respectively, and fill to obtain blue ceramic inkjet ink.
[0049] The ceramic inkjet ink prepar...
Embodiment 2
[0065] Embodiment 2-a kind of production technology of novel ceramic ink-jet ink, comprises the steps:
[0066] (1) Weigh 40% of soluble metal salt, 14% of surfactant and 9% of complexing agent in proportion, dissolve them with 40% of water-soluble organic solvent, put them into the reaction kettle for heating reaction, After cooling, the residue was removed by filtration;
[0067] Wherein: the soluble metal salt is a combination of chromium sulfate, chromium acetate and chromium chloride; the surfactant is dodecylphenyl acid; the complexing agent is sodium sulfate and EDTA; the water-soluble organic solvent is Ethanol and butanol account for 32% of the ink solution; excipients account for 2% of the ink solution.
[0068] (2) Add dispersant to the reaction kettle in step (1), and add 0.06% pH regulator to adjust the pH value to 7;
[0069] (3) Put the remaining 60% water-soluble organic solvents and additives into the reaction solution for reaction;
[0070] (4) After compl...
Embodiment 3
[0072] Embodiment 3 A kind of production technology of novel ceramic ink-jet ink, comprises the steps:
[0073] (1) Weigh 42% of soluble metal salt, 14% of surfactant and 8% of complexing agent in proportion, dissolve them with 50% of water-soluble organic solvent, put them into the reaction kettle for heating reaction, After cooling, the residue was removed by filtration;
[0074] Wherein: the soluble metal salt is a combination of zinc sulfate, zinc acetate and zinc chloride; the surfactant is sodium citrate and ammonium citrate; the complexing agent is potassium phosphate and caustic soda; the water-soluble organic solvent It is butanol, accounting for 30% of the ink solution; auxiliary materials account for 3% of the ink solution.
[0075] (2) Add dispersant to the reaction kettle in step (1), and add 0.08% pH regulator to adjust the pH value to 7;
[0076] (3) Put the remaining 50% water-soluble organic solvents and additives into the reaction solution for reaction;
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