Preparation process of low modulus waterproof silicone sealing material

A sealing material and preparation process technology, applied in other chemical processes, chemical instruments and methods, etc., can solve the problems of extrusion damage, neglect of multi-functional requirements, insufficient displacement ability, etc., and achieve excellent high and low temperature resistance, excellent The effect of stretch recovery and high elongation at break

Pending Publication Date: 2016-11-02
西安亚岱新能源科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These materials have poor aging resistance, short service life, low adhesion and strength to the substrate, insufficient displacement capacity, and are prone to problems such as disengagement, fracture, extrusion damage, etc., and most of them are toxic and easy to cause environmental pollution.
Silicone materials are excellent in waterproofing, economical, convenient in construction, and do not change the appearance of concrete structures, so they have received extensive attention. However, many studies and patents simply focus on waterproofing, ignoring the multifunctional requirements of building materials such as environmental protection.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0012] The preparation process of the low modulus waterproof silicone sealing material is completed through the following steps:

[0013] (1) Disperse 5 parts of polymethyltriethoxysiloxane into 25 parts of organosilane coupling agents containing cyano groups, and stir evenly to obtain a mixed solution;

[0014] (2) Add 30 parts of superfine activated calcium carbonate, 3 parts of diketoxime silane and 3 parts of ketoxime silane into the mixed solution, and mix uniformly for 10 minutes under vacuum condition;

[0015] (3) Add 1 part of organic tin carboxylate and chelate compound thereof in the mixed solution obtained in step 2, and mix evenly for 10 minutes again;

[0016] (4) Vacuum the mixed liquid to remove air bubbles, and remove part of the low-molecular substances generated in the reaction at the same time to obtain a low-modulus waterproof silicone sealing material.

Embodiment 2

[0018] The preparation process of the low modulus waterproof silicone sealing material is completed through the following steps:

[0019] (1) Disperse 10 parts of methyl-terminated polydimethylsiloxane into 35 parts of organosilane coupling agent containing secondary amino groups, and stir evenly to obtain a mixed solution;

[0020] (2) Add 40 parts of superfine activated calcium carbonate, 5 parts of diketoxime polysiloxane and 5 parts of ketoxime polysiloxane into the mixed solution, and mix uniformly for 20 minutes under vacuum condition;

[0021] (3) Add 3 parts of organic titanate and chelate compound thereof to the mixed solution obtained in step 2, and mix uniformly again for 20 minutes;

[0022] (4) Vacuum the mixed liquid to remove air bubbles, and remove part of the low-molecular substances generated in the reaction at the same time to obtain a low-modulus waterproof silicone sealing material.

[0023] After testing, the low-modulus waterproof silicone sealing mater...

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PUM

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Abstract

The invention discloses a preparation process of a low-modulus waterproof organic silicon sealing material, which comprises the following steps: (1) dispersing 5-10 parts of organic silicon oligomers into 25-35 parts of organic silane coupling agent, stirring evenly to obtain Mixed solution; (2) Add 30-40 parts of filler, 3-5 parts of chain extender and 3-5 parts of crosslinking agent to the mixed solution, and mix uniformly for 10-20 minutes under vacuum; (3) Obtained in step 2 Add 1-3 parts of catalyst to the mixed solution, and mix uniformly again for 10-20 minutes; (4) Vacuum the mixed solution to remove air bubbles, and at the same time remove part of the low-molecular substances generated in the reaction to obtain low-modulus waterproof silicone Sealing material. The organosilicon sealing material of the present invention has excellent high and low temperature resistance, good water resistance, excellent stretch recovery, low modulus, and high elongation at break, and can be used for waterproofing of hydraulic concrete, anticorrosion of marine concrete, and road concrete Among materials such as protective materials, it has the advantages of non-toxic, harmless and non-polluting to the environment.

Description

technical field [0001] The invention relates to a preparation method of a polymer material, in particular to a preparation process of a low-modulus waterproof organic silicon sealing material. Background technique [0002] With the rapid development of construction and transportation in my country, large-scale construction facilities, highways and tunnel projects are increasing day by day. The problem of concrete expansion joints has attracted great attention from the engineering community. It is required to further improve the aging resistance, water resistance and elasticity of concrete expansion joint materials. performance, overall adhesion and strength. At present, the concrete joint sealing materials used in China mainly include asphalt, modified asphalt, prefabricated neoprene rubber, polysulfide and polyurethane. These materials have poor aging resistance, short service life, low adhesion and strength to the substrate, insufficient displacement capacity, and are pron...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L83/04C08L83/06C08K9/04C08K3/26C08K5/544C08J3/24C09K3/10
Inventor 韩英
Owner 西安亚岱新能源科技有限公司
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