Preparation of extreme pressure anti-wearing additive and energy-saving environmental-friendly engine oil containing same
An extreme pressure anti-wear agent, energy saving and environmental protection technology, applied in additives, petroleum industry, lubricating composition, etc., can solve problems such as redox catalyst poisoning failure, catalyst poisoning, reduced catalytic effect, etc., to achieve good wear resistance, Good bearing capacity and extreme pressure resistance, the effect of improving wear resistance
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Embodiment 1
[0030] This embodiment provides a preparation method of an extreme pressure antiwear agent, and an energy-saving and environment-friendly engine oil containing the extreme pressure antiwear agent.
[0031] A preparation method of an extreme pressure antiwear agent, specifically comprising the following steps:
[0032] a. Dissolve 60g of lanthanum bromide in distilled water and stir until clear liquid;
[0033] b. Add dropwise an ethanol solution containing 160g of graphene modified by polymerized ionic liquids and 30g of sodium carbonate under vigorous stirring, the solution is immediately white and turbid, reacted at constant temperature for 1h, and the reaction is complete;
[0034] c. Set aside for sedimentation, filter, wash with distilled water for several times, and then wash with absolute ethanol for 10 times;
[0035] d. Finally, wash with potassium tetrafluoroborate aqueous solution for 10 times, carry out particle exchange, dry the sample, and grind it finely for la...
Embodiment 2
[0038] This embodiment provides a preparation method of an extreme pressure antiwear agent, and an energy-saving and environment-friendly engine oil containing the extreme pressure antiwear agent.
[0039] A preparation method of an extreme pressure antiwear agent, specifically comprising the following steps:
[0040] a. Dissolve 65g of lanthanum bromide in distilled water and stir until clear liquid;
[0041] b. Add dropwise an ethanol solution containing 170g of graphene modified by polymerized ionic liquids and 35g of sodium carbonate under vigorous stirring, the solution is immediately white and turbid, and reacted at constant temperature for 2 hours, and the reaction is complete;
[0042] c. Set aside to settle, filter, wash with distilled water for several times, and then wash with absolute ethanol for 15 times;
[0043] d. Finally, wash with potassium tetrafluoroborate aqueous solution for 12 times, carry out particle exchange, dry the sample, and grind it finely for l...
Embodiment 3
[0046] This embodiment provides a preparation method of an extreme pressure antiwear agent, and an energy-saving and environment-friendly engine oil containing the extreme pressure antiwear agent.
[0047] A preparation method of an extreme pressure antiwear agent, specifically comprising the following steps:
[0048] a. Dissolve 70g of lanthanum bromide in distilled water and stir until clear liquid;
[0049] b. Add dropwise an ethanol solution containing 180g of graphene modified by polymerized ionic liquids and 40g of sodium carbonate under vigorous stirring, the solution is immediately white and turbid, reacted at constant temperature for 3 hours, and the reaction is complete;
[0050] c. Set aside for sedimentation, filter, wash with distilled water several times for precipitation, and then wash 20 times with absolute ethanol;
[0051] d. Finally, wash with potassium tetrafluoroborate aqueous solution for 15 times, carry out particle exchange, dry the sample, and grind it ...
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