Black rice extract, preparing method thereof and application thereof to cosmetics
An extract and cosmetic technology, applied in the field of black rice extract and its preparation, can solve the problems of clogged pores, enlarged pores, blackheads, etc., and achieve the effects of good anti-aging ability, maintaining skin elasticity, and promoting secretion
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Embodiment 1
[0046]Get 10kg of dried black rice, wash twice with deionized water and blow dry with hot air, pulverize, and pass 80 mesh sieves, add the black rice after sieving to a tower kettle volume of 150L, be equipped with a diameter of 5mm θ ring rectification In the column, the theoretical plate number of the rectification column is 20. The feed inlet is set on the 5th layer, 100L of deionized water is added to the tower kettle from the feed inlet, soaked for 2 hours, the pressure of the rectification tower is adjusted to 0.8MPa, the tower kettle is heated and boiled, and kept boiling for 2 hours, and the reflux ratio at the top of the tower is set. is 5, the flow rate of the feed port is 3L / min, the extraction liquid is continuously produced from the tower kettle, and the deionized water produced at the top of the tower is returned to the solvent tank for recycling. The extract was concentrated to 20% of the original volume at 5 kPa and 30°C to obtain a concentrated solution.
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Embodiment 2
[0050] Get 10kg of dried black rice, wash twice with deionized water and blow dry with hot air, pulverize, and pass through a 60 mesh sieve, add the sieved black rice to a tower kettle with a volume of 250L and be equipped with a rectification of a 5mm θ ring in diameter. In the column, the theoretical plate number of the rectification column is 15. The feed inlet is located on the 7th layer, and 200L of 70% methanol solution is added to the tower kettle from the feed inlet, soaked for 2 hours, the tower kettle is heated and boiled, and kept boiling for 2 hours, the reflux ratio at the top of the tower is set to 5, and the flow rate of the feed inlet At 5L / min, the extraction liquid is continuously extracted from the tower kettle, and the methanol extracted at the top of the tower is returned to the solvent tank for recycling.
[0051] Adjust the pH value of the extraction solution = 4, use ADS-5 macroporous adsorption resin to adsorb to saturation, use deionized water, 20% et...
Embodiment 3
[0054] Take 10kg of dried black rice, wash it twice with deionized water, dry it with hot air, pulverize it, pass it through an 80-mesh sieve, add the sieved black rice to the extraction tower, then add 50L of deionized water to it, soak for 2 hours , heated and boiled under a pressure of 1.1MPa, and kept boiling for 2h to obtain extract 1, then added 100L of chloroform to the remaining residue, heated and boiled under a pressure of 1.1MPa, and kept boiling for 2h to obtain extract 2, mixed and extracted Liquid one and extract two, respectively concentrate extract one and extract two to 30% of the added volume, and then use ADS-5 macroporous adsorption resin to adsorb the concentrated extract one and extract two to saturation respectively, and then respectively. Use deionized water, 30% ethanol solution, and 60% ethanol solution to elute the macroporous adsorption resin, mix the eluents, and concentrate under reduced pressure at 10KPa and 45°C, recover the ethanol, and dry the ...
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