A kind of amorphous alloy powder and preparation method thereof
A technology of amorphous alloys and iron-based amorphous alloys, applied in the direction of inorganic materials, magnetic objects, magnetic materials, etc., can solve the problems of unfavorable preparation performance of magnetic powder cores, and achieve crystallization transformation and uniform stress release, particle length and width Uniform, particle size-optimized results
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Embodiment 1
[0039] This embodiment provides an amorphous alloy powder and a preparation method thereof, and the corresponding preparation method includes the following steps:
[0040] S1. Using a mechanical crusher, the thickness is 18μm, the bandwidth is 10mm, and the composition is Fe 80 Si 9 B 11 The iron-based amorphous alloy thin strips are broken into fragments of 50 mesh to 200 mesh;
[0041] S2. Under a nitrogen protective atmosphere, put the amorphous fragments obtained after the crushing treatment into an atmosphere rotary furnace, and heat-treat at 300°C for 1h. During the heat treatment, control the rotation rate of the atmosphere rotary furnace to 5r / min and the atmosphere pressure 0.1MPa, keep turning the atmosphere rotary furnace, so that the amorphous fragments are evenly heated;
[0042] S3. Put the heat-treated amorphous fragments into the airflow grinder, control the output power of the airflow grinder to 35KW, and grind for 50min to realize the optimization of the p...
Embodiment 2
[0050] This embodiment provides an amorphous alloy powder and a preparation method thereof, and the corresponding preparation method includes the following steps:
[0051] S1. Using a mechanical crusher, the thickness is 20μm, the bandwidth is 20mm, and the composition is Fe 78 Si 9 B 13 The iron-based amorphous alloy thin strips are broken into fragments of 50 mesh to 200 mesh;
[0052] S2. Under a nitrogen protective atmosphere, put the amorphous fragments obtained after the crushing treatment into an atmosphere rotary furnace, and heat-treat at 300°C for 1h. During the heat treatment, control the rotation rate of the atmosphere rotary furnace to 10r / min and the atmosphere pressure 0.2MPa, keep turning the atmosphere rotary furnace, so that the amorphous fragments are evenly heated;
[0053] S3. Put the heat-treated amorphous fragments into the airflow grinder, control the output power of the airflow grinder to 70KW, and grind for 50min to realize the optimization of the ...
Embodiment 3
[0059] This embodiment provides an amorphous alloy powder and a preparation method thereof, and the corresponding preparation method includes the following steps:
[0060] S1. Using a mechanical crusher, the thickness is 25μm, the bandwidth is 30mm, and the composition is Fe 80 Si 9 B 11 The iron-based amorphous alloy thin strips are broken into fragments of 50 mesh to 200 mesh;
[0061] S2. Under a nitrogen protective atmosphere, put the amorphous fragments obtained after the crushing treatment into an atmosphere rotary furnace, and heat-treat at 280°C for 1h. During the heat treatment, control the rotation rate of the atmosphere rotary furnace to 20r / min and the atmosphere pressure 0.3MPa, keep turning the atmosphere rotary furnace, so that the amorphous fragments are evenly heated;
[0062] S3. Put the heat-treated amorphous fragments into the airflow grinder, control the output power of the airflow grinder to 50KW, and grind for 60min to realize the optimization of the ...
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Abstract
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