PP melt-blown filter element based on modified bentonite and preparation method thereof
A melt-blown filter element and bentonite technology, applied in separation methods, chemical instruments and methods, filtration separation, etc., can solve problems such as breeding microorganisms, filtering liquid pollution, and limiting the development of PP filter elements
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[0017] The present invention provides a kind of preparation method based on bentonite modified PP melt-blown filter element, comprising:
[0018] 1) spraying the polymer coating on the surface of bentonite, then drying, soaking in dilute sulfuric acid solution, and filtering to obtain activated bentonite;
[0019] 2) spray the silver nitrate solution and the hydrazine sulfate solution on the surface of the activated bentonite at the same time, and let it stand to prepare the silver-modified bentonite;
[0020] 3) decocting and filtering the Chinese herbal medicine in water to obtain the Chinese herbal medicine extract and the Chinese herbal medicine filter cake;
[0021] 4) In the presence of protective gas, place the silver-modified bentonite at 240-255° C. for calcination for 25-40 minutes, and then place the calcined product in Chinese herbal medicine extract for impregnation and filtration to obtain Chinese herbal medicine-modified bentonite;
[0022] 5) PP (polypropylene...
Embodiment 1
[0041] 1) Polymer coating (containing polyvinyl alcohol, 1.2% by weight of p-aminophenol platinum, 0.7% by weight of palladium (II)-2-(5-bromo-2-pyridylazo)-5-diethylaminophenol ) is sprayed on the surface of bentonite, then dried at 125°C for 6h, placed in 50°C and 18% by weight dilute sulfuric acid solution, soaked for 2h, and filtered to obtain activated bentonite, wherein the bentonite, polymer coating, dilute sulfuric acid solution The weight ratio is 100:4:200;
[0042] 2) Spray 5% by weight of silver nitrate solution and 2.5% by weight of hydrazine sulfate solution on the surface of activated bentonite at the same time, and leave it at 30°C for 5 hours to obtain silver-modified bentonite, wherein activated bentonite, silver nitrate solution, and hydrazine sulfate The weight ratio of the solution is 100:7:11;
[0043] 3) Combine lemongrass, Artemisia annua, licorice, flavescens, fennel, Poria bark, red peony root, red euphorbia, Magnolia officinalis and water according ...
Embodiment 2
[0047] 1) Polymer coating (containing polyvinyl alcohol, 0.8% by weight of p-aminophenol platinum, 0.2% by weight of palladium (II)-2-(5-bromo-2-pyridylazo)-5-diethylaminophenol ) is sprayed on the surface of bentonite, then dried at 120°C for 5h, placed in 45°C and 15% by weight of dilute sulfuric acid solution, soaked for 1h, and filtered to obtain activated bentonite, wherein the bentonite, polymer coating, dilute sulfuric acid solution The weight ratio is 100:3:150;
[0048] 2) Simultaneously spray 4% by weight of silver nitrate solution and 2% by weight of hydrazine sulfate solution on the surface of activated bentonite, and leave it at 25°C for 4h to obtain silver-modified bentonite, wherein activated bentonite, silver nitrate solution, hydrazine sulfate The weight ratio of the solution is 100:5:10;
[0049] 3) Combine lemongrass, Artemisia annua, licorice, flavescens, fennel, Poria bark, red peony root, red euphorbia, Magnolia officinalis and water according to the rat...
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