Preparation method of low temperature graphite anode material for lithium ion battery
A lithium-ion battery, graphite negative electrode technology, applied in battery electrodes, graphene, circuits, etc., can solve the problems of inability to adapt to low-temperature operation of lithium-ion batteries, and can not effectively solve low-temperature lithium intercalation of graphite, etc. Small, highly isotropic effects
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[0020] Example 1
[0021] A preparation method of low-temperature graphite negative electrode material for lithium ion batteries includes the following steps:
[0022] 1) Disperse graphite, dispersant, and the first carbon source in a water-soluble solvent, and mix 0.5 by ultrasonic to obtain a mixed solution; the first carbon source is a mixture of glucose and phenolic resin in a mass ratio of 1:1; The graphite is natural graphite with a particle size D50=10um; the water-soluble solvent is distilled water; and the dispersant is polyvinylpyrrolidone.
[0023] 2) Grind the mixed liquid obtained in step (1) with a sand mill for 5 hours at a grinding speed of 500r / min, and then add a water-soluble solvent to make the solid content in the mixed liquid 5%;
[0024] 3) Dry the ground mixture in step (2) into powder using a spray dryer to obtain agglomerated granules. The inlet air temperature of the spray drying is 300°C, the outlet air temperature is 150°C, and the constant current pump sp...
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[0027] Example 2
[0028] A preparation method of low-temperature graphite negative electrode material for lithium ion batteries includes the following steps:
[0029] 1) Disperse graphite, dispersant, and first carbon source in a water-soluble solvent, and mix them by ultrasonic for 2 hours to obtain a mixed solution; the first carbon source is a mixture of glucose and phenolic resin at a mass ratio of 1:1; The graphite is natural graphite with a particle size D50=1um; the water-soluble solvent is ethanol; and the dispersant is sodium lauryl sulfate.
[0030] 2) Grind the mixed liquid obtained in step (1) with a sand mill for 1 hour at a grinding speed of 2500r / min, and then add a water-soluble solvent to make the solid mass content in the mixed liquid 20%;
[0031] 3) Dry the ground mixture in step (2) into powder using a spray dryer to obtain agglomerated granules. The inlet air temperature of spray drying is 200°C, the outlet air temperature is 100°C, and the constant current pump...
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[0034] Example 3
[0035] A preparation method of low-temperature graphite negative electrode material for lithium ion batteries includes the following steps:
[0036] 1) Disperse graphite, dispersant, and the first carbon source in a water-soluble solvent, and mix them by ultrasonic for 1.5 hours to obtain a mixed solution; the first carbon source is a mixture of polyvinyl alcohol and furfural resin at a mass ratio of 1:1 The graphite is artificial nitrograph, particle size D50=5um; the water-soluble solvent is a mixture of distilled water and ethylene glycol at a molar ratio of 1:1; the dispersant is polyvinylpyrrolidone and polyethyleneimine at a molar ratio of 1:1 1 mixed.
[0037] 2) Grind the mixed liquid obtained in step (1) with a sand mill for 3 hours at a grinding speed of 1500r / min, and then add a water-soluble solvent to make the solid mass content in the mixed liquid 10%;
[0038] 3) Dry the ground mixture in step (2) into powder using a spray dryer to obtain agglomerate...
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