Preparation method of sponge structure iron/SiC particle-based oil-water separation enhancement layer material

An oil-water separation and structural technology, which is applied in the field of preparation of sponge structure iron/SiC particle-based oil-water separation enhancement layer materials, can solve problems such as secondary environmental pollution, and achieve strong adsorption, strong drainage, and oil-water separation efficiency. high effect

Active Publication Date: 2017-01-04
山东清大银光金属海绵新材料股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The separation efficiency of these treatment technologies needs to be improved, and some of them need to add chemical agents, thus causing secondary pollution to the environment

Method used

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  • Preparation method of sponge structure iron/SiC particle-based oil-water separation enhancement layer material
  • Preparation method of sponge structure iron/SiC particle-based oil-water separation enhancement layer material

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Embodiment 1

[0032] Preferred Embodiment 1 of the present invention provides a method for preparing a sponge-structured iron / SiC nanoparticle composite material, comprising the following steps in order:

[0033] ① Conductive treatment of polyurethane sponge model: Mix nano-carbon powder, nano-iron powder, ethyl hydroxyethyl cellulose, xanthan gum, sodium silicate and deionized water to form a conductive paste. The mass percentages of each component in the above-mentioned conductive paste are respectively: nano-carbon powder 18%, nano-iron powder 20%, ethyl hydroxyethyl cellulose 3%, xanthan gum 5%, ammonium bicarbonate 1.5%, and the rest are Deionized water; After fully soaking the polyurethane sponge in the conductive paste, dry it in a 35°C drying oven for 4 hours to obtain a conductive polyurethane sponge model.

[0034] ② Sponge structure type iron / SiC nanoparticle matrix composite electrodeposition treatment: the concentration is analytically pure iron oxide, hydrochloric acid with a ...

Embodiment 2

[0038] Preferred embodiment 2 of the present invention provides a method for preparing a sponge-structured iron / SiC nanoparticle composite material with reduced surface energy, comprising the following steps in order:

[0039] ① Conductive treatment of polyurethane sponge model: Mix nano-carbon powder, nano-iron powder, ethyl hydroxyethyl cellulose, xanthan gum, sodium silicate and deionized water to form a conductive paste. The mass percentages of each component in the above-mentioned conductive paste are respectively: nano-carbon powder 18%, nano-iron powder 20%, ethyl hydroxyethyl cellulose 3%, xanthan gum 5%, ammonium bicarbonate 1.5%, and the rest are Deionized water; After fully soaking the polyurethane sponge in the conductive paste, dry it in a 35°C drying oven for 4 hours to obtain a conductive polyurethane sponge model.

[0040] ② Sponge structure type iron / SiC nanoparticle matrix composite electrodeposition treatment: the concentration is analytically pure iron oxid...

Embodiment 3

[0045] Preferred embodiment 3 of the present invention provides a preparation method of a sponge-structured iron / SiC nanoparticle-based superhydrophobic / superoleophilic reinforcement layer oil-water separation material, comprising the following steps in order:

[0046] ① Conductive treatment of polyurethane sponge model: Mix nano-carbon powder, nano-iron powder, ethyl hydroxyethyl cellulose, xanthan gum, sodium silicate and deionized water to form a conductive paste. The mass percentages of each component in the above-mentioned conductive paste are respectively: nano-carbon powder 18%, nano-iron powder 20%, ethyl hydroxyethyl cellulose 3%, xanthan gum 5%, ammonium bicarbonate 1.5%, and the rest are Deionized water; After fully soaking the polyurethane sponge in the conductive paste, dry it in a 35°C drying oven for 4 hours to obtain a conductive polyurethane sponge model.

[0047] ② Sponge structure type iron / SiC nanoparticle matrix composite electrodeposition treatment: the c...

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Abstract

The invention relates to a preparation method of a sponge structure iron/SiC particle-based oil-water separation enhancement layer material capable of being applied to separation treatment of oily sewage on a large scale. The preparation method comprises the steps of preparing a sponge structure iron/SiC nano particle matrix through composite electrodeposition; and preparing a SiC nano particle super-hydrophobic/super-oleophylic enhancement layer on the surface of the matrix through etching/modification. The method specifically comprises the processes of (1) composite electrodeposition of the sponge structure iron/SiC nano particle matrix; (2) surface etching of the sponge structure iron/SiC nano particle matrix; and (3) surface super-hydrophobic/super-oleophylic modification of the sponge structure iron/SiC nano particle matrix. A novel oil-water separation material prepared through the method has the characteristics that the specific surface area is large, the oil and water separation efficiency is high, and the separation treatment process of the oily sewage is environment-friendly, and can be applied to separation treatment of oily sewage on a large scale.

Description

technical field [0001] The invention relates to the field of oil-water separation materials, in particular to a method for preparing a sponge-structured iron / SiC particle-based oil-water separation enhancement layer material. Background technique [0002] With the development of the economy, oily sewage pollution caused by oil production sewage, catering sewage, and marine oil spill pollution has become more and more serious, and has seriously threatened the safety of human beings and the ecological environment. Therefore, the treatment of oily sewage is an urgent problem to be solved. Traditional methods for treating oily wastewater include: gravity separation, biological treatment, chemical treatment, and gas removal. The separation efficiency of these treatment technologies needs to be improved, and some of them need to add chemical agents, thus causing secondary pollution to the environment. Therefore, it is of great significance to develop environmentally friendly new...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C25D15/00B01D17/022
CPCB01D17/02C25D15/00
Inventor 李建国赵明
Owner 山东清大银光金属海绵新材料股份有限公司
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