High-temperature-resistant and salt-resistant filtrate loss reducer for drilling fluid and preparation method and application of filtrate loss reducer

A technology of fluid loss reducer and drilling fluid, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of high price, high temperature resistance, salt resistance limitation, long reaction time, etc., and achieve high performance stable effect

Inactive Publication Date: 2017-02-01
YANGTZE UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Although there are many types of fluid loss control agents used in oilfield drilling, there are few products that have good temperature resistance and salt resistance at the same time.
The preparation method of the anti-high temperature and anti-salt fluid loss reducer disclosed in the patent document CN104292387A is: adjust the aqueous solution of 2-acrylamide-2-methylpropanesulfonic acid to 7, and then add acrylamide and diallyl Aqueous solution of dimethyl ammonium chloride, pass nitrogen gas and stir to obtain a mixed solution, add initiator to the mixed solution, let it stand at 35-55°C for 3-7 hours, wash the viscous material repeatedly with ethanol, and dry it High-temperature and salt-resistant fluid loss additives are obtained, but the defect in the preparation method of fluid loss additives in the prior art is that the high-temperature and salt-resistant properties of the fluid loss additive products have certain limitations, and the reaction time Longer, more complex processing technology, expensive

Method used

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  • High-temperature-resistant and salt-resistant filtrate loss reducer for drilling fluid and preparation method and application of filtrate loss reducer
  • High-temperature-resistant and salt-resistant filtrate loss reducer for drilling fluid and preparation method and application of filtrate loss reducer
  • High-temperature-resistant and salt-resistant filtrate loss reducer for drilling fluid and preparation method and application of filtrate loss reducer

Examples

Experimental program
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Effect test

Embodiment 1

[0032] A high-temperature and salt-resistant fluid loss reducer for drilling fluid, the preparation method of which is as follows:

[0033] (1) Add 10 parts of 2-acrylamide-2-methylpropanesulfonic acid and 20 parts of water into the reactor, stir to fully dissolve 2-acrylamide-2-methylpropanesulfonic acid in water;

[0034] (2) Add 10 parts of acrylic acid to the aqueous solution of 2-acrylamide-2-methylpropanesulfonic acid to form a mixture A, then add a pH regulator to the mixture A, and adjust the pH value of the mixture A to 7;

[0035] (3) Heating the reactor so that the temperature of the mixture A in the reactor is maintained at 45°C, then adding 4 parts of N-isopropylacrylamide and 3.5 parts of nano-calcium bentonite to the mixture A, and stirring evenly to obtain the mixture B;

[0036] (4) Add 0.7 parts of initiator to the mixture B, and react for 60 min at 45° C. to obtain a reaction product;

[0037] (5) washing the reaction product obtained in step (4) with aceto...

Embodiment 2

[0040] A high-temperature and salt-resistant fluid loss reducer for drilling fluid, the preparation method of which is as follows:

[0041] (1) Add 2 parts of 2-acrylamide-2-methylpropanesulfonic acid and 25 parts of water into the reactor, stir to fully dissolve 2-acrylamide-2-methylpropanesulfonic acid in water;

[0042] (2) Add 15 parts of acrylic acid to the aqueous solution of 2-acrylamide-2-methylpropanesulfonic acid to form a mixture A, then add a pH regulator to the mixture A, and adjust the pH value of the mixture A to 8;

[0043] (3) Heating the reactor so that the temperature of the mixture A in the reactor is maintained at 40° C., then adding 3 parts of N-isopropylacrylamide and 2.5 parts of nano-calcium bentonite to the mixture A, and stirring evenly to obtain the mixture B;

[0044] (4) Add 0.6 parts of initiator to the mixture B, and react for 70 minutes at 40° C. to obtain a reaction product;

[0045] (5) washing the reaction product obtained in step (4) with ...

Embodiment 3

[0048] A high-temperature and salt-resistant fluid loss reducer for drilling fluid, the preparation method of which is as follows:

[0049] (1) Add 20 parts of 2-acrylamide-2-methylpropanesulfonic acid and 45 parts of water into the reactor, stir to fully dissolve 2-acrylamide-2-methylpropanesulfonic acid in water;

[0050] (2) Add 20 parts of acrylic acid to the aqueous solution of 2-acrylamide-2-methylpropanesulfonic acid to form a mixture A, then add a pH regulator to the mixture A, and adjust the pH value of the mixture A to 9;

[0051] (3) Heating the reactor so that the temperature of the mixture A in the reactor is maintained at 50° C., then adding 4 parts of N-isopropylacrylamide and 7 parts of nano-calcium bentonite to the mixture A, and stirring evenly to obtain the mixture B;

[0052] (4) Add 0.7 parts of initiator to the mixture B, and react for 50 minutes at 50° C. to obtain a reaction product;

[0053] (5) washing the reaction product obtained in step (4) with ace...

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Abstract

The invention discloses a high-temperature-resistant and salt-resistant filtrate loss reducer for drilling fluid and a preparation method and application of the filtrate loss reducer. The preparation method comprises the following steps that 2-acrylamido-2-methylpropane sulfonic acid and water are added into a reactor and stirred to be fully dissolved; acrylic acid is added into the reactor, then a pH value regulator is added, and the pH value of the mixture in the reactor is regulated to be 7-9; N-isopropylacrylamide and nano-calcium bentonite are added into the reactor and stirred to be uniform; an initiator is added into the reactor, and a reaction is conducted to obtain a reaction product; the obtained reaction product is washed with acetone, filtration is conducted, and then a filtration product is collected; the filtration product is dried in vacuum and then crushed to obtain white powder, that is, the high-temperature-resistant and salt-resistant filtrate loss reducer for the drilling fluid. The filtrate loss reducer prepared through the method is good in performance and temperature-resistant and salt-resistant effect, simple in processing technology and low in development cost.

Description

technical field [0001] The invention relates to the technical field of fluid loss control agents using organic molecules as raw materials. More specifically, it relates to a high-temperature and salt-resistant fluid loss reducer for drilling fluid, a preparation method and application thereof. Background technique [0002] When drilling or completing a well in a formation, various fluids are typically used in the well for a variety of reasons. Common uses of well fluids include: wetting and cooling drill bit cutting surfaces during normal drilling or drill-out (drilling through targeted oil-bearing formations); transport to the surface; control formation fluid pressure to prevent blowout; maintain well stability; suspend solids in the well; minimize fluid loss in the drilling formation and stabilize formations drilled through; fracture the formation near the well, Substituting another fluid for the fluid in the well; cleaning the well; testing the well; transmitting hydrau...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08F220/58C08F220/06C08F220/54C08K3/34C09K8/035C09K8/24
CPCC08F220/06C08F220/58C08F220/585C08K3/346C09K8/035C09K8/24C08F220/54
Inventor 王松张桂强李红田茂明胡三清郑文武李行
Owner YANGTZE UNIVERSITY
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