Nasal mask for OSA patient
A nasal mask, patient technology
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Embodiment 1
[0031] like figure 1 As shown, a nasal mask for OSA patients comprises a bracket 1, and the two ends of the bracket 1 are respectively fixedly connected with a nose piece 2, and the nose piece 2 is provided with a ventilation tube 3, the inside of the nose piece 2 and the bracket 1 are hollow, and the ventilation tube 3 It communicates with the inside of the nose piece 2 and the bracket 1, the bracket 1 is made of flexible material, and the inside of the bracket 1 is provided with a shaped iron wire. The middle part of the support 1 is provided with a connecting through hole, and the connecting through hole runs through the upper and lower surfaces of the support 1 . The connection through hole is connected with the air delivery pipe 7 , and the air delivery pipe 7 is arranged on the upper surface side of the support 1 , and the front end of the air delivery pipe 7 passes through the connection through hole and is connected with the gasket 5 . Air holes 8 are evenly distribut...
Embodiment 2
[0037] The preparation method of crotonate-grafted starch is as follows,
[0038] Step 1: Weigh a portion of starch, take an appropriate amount of water as a solvent, adjust the pH of the solution to 4.7, add an appropriate amount of isopropanol to prepare a suspension with a starch mass fraction of 37%, and stir for 30 minutes;
[0039] Step 2: Add NaOH to the solution according to the starch:NaOH mass ratio of 1:0.05, heat up to 30°C, stir at a constant temperature for 30 minutes, and slowly drop allyl chloride into the solution according to the NaOH:allyl chloride molar ratio of 1:1.2 , heated up to 50°C, and stirred at constant temperature for 24h;
[0040]Step 3: Filtration, taking the solid and redispersing it in a distilled water-ethanol solution with a volume ratio of 18:82, adjusting the pH to 7 with acetic acid, washing with an appropriate amount of distilled water after suction filtration, and drying to obtain allyl etherified starch;
[0041] Step 4: Take a portio...
Embodiment 3
[0044] Pseudoephedrine derivatives The synthesis method is as follows:
[0045]
[0046] Reagents and conditions: (Ia-i) periodate, chromium trioxide, glucose isomerase, acetonitrile, room temperature; (Ia-ii) sodium hydride, ethanol, α-amylase, room temperature; (Ia-iii) hydroboration Sodium, DMF, heated to reflux; (Ia-iv) sodium ethoxide, DMF, heated to reflux.
[0047] Weigh 1.71g of 2-(5-chloro-2-methylphenyl)ethan-1-ol into a 150mL three-neck flask, measure 20mL of acetonitrile, stir and dissolve at room temperature, add 0.4g of glucose isomerase , 0.2g of chromium trioxide, continue to stir at room temperature for 10min, weigh 2.28g of periodic acid and dissolve in 10mL of acetonitrile, gradually and slowly dropwise add to the reaction system, and continue to react at room temperature for 36h. After the reaction of Ia-1 was completed, the reaction was stopped, and the solvent was concentrated under reduced pressure. Through column chromatography, the developer was ...
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