A kind of rare earth strontium aluminate long afterglow light-emitting fiber with skin-core structure and preparation method thereof
A light-emitting fiber, skin-core structure technology, applied in fiber processing, fiber chemical characteristics, melt spinning, etc., can solve the problems of low mechanical properties, poor water resistance of light-emitting fibers, etc., achieve smooth surface, improve light-emitting effect, and ensure light-emitting brightness. Effect
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Embodiment 1
[0024] In the rare earth strontium aluminate long-lasting luminous fiber with a skin-core structure in this embodiment, the core layer accounts for 70% and the skin layer accounts for 30% by mass fraction; wherein, the core layer is made of the following raw materials in weight percentage:
[0025] PA6 89.46%, rare earth strontium aluminate 10%, phosphite 0.02%, antioxidant 1010 0.01%, antioxidant 1680.01%, KH-560 silane coupling agent 0.5%; the skin layer is made of polyphenylene, which accounts for 29.6% of the total mass of the luminous fiber Ethylene and toughener A-662 accounted for 0.4% of the total mass of the luminous fiber.
[0026] The steps of the preparation method of the rare earth strontium aluminate long-lasting luminous fiber with skin-core structure in this embodiment are as follows:
[0027] (1) Preparation of PA6 luminescent masterbatch: 89.46% of PA6 slices, 10% of rare earth strontium aluminate, 0.02% of phosphite, 0.01% of antioxidant 1010 and 168, and 0....
Embodiment 2
[0032] The rare earth strontium aluminate long-lasting luminescent fiber with a skin-core structure in this embodiment has a core layer accounting for 80% and a skin layer accounting for 20% by mass fraction; wherein, the core layer is made of the following raw materials in weight percentage:
[0033] 79.09% of PA6, 20% of rare earth strontium aluminate, 0.03% of phosphite, 0.04% of antioxidant 1010 and 0.04% of antioxidant 168, 0.8% of KH-560 silane coupling agent; Methyl methacrylate and toughening agent A-608 accounting for 0.3% of the total mass of the luminescent fiber.
[0034] The steps of the preparation method of the rare earth strontium aluminate long-lasting luminous fiber with skin-core structure in this embodiment are as follows:
[0035] (1) Preparation of PA6 luminescent masterbatch: 79.09% of PA6 slices, 20% of rare earth strontium aluminate, 0.03% of phosphite, 0.04% of antioxidant 1010 and 168, and 0.8% of KH-560 silane coupling agent are used at high speed ...
Embodiment 3
[0040] In the rare earth strontium aluminate long-lasting luminous fiber with a skin-core structure in this embodiment, the core layer accounts for 85% and the skin layer accounts for 15% by mass fraction; wherein, the core layer is made of the following raw materials in weight percentage:
[0041]68.8% of PA6, 30% of rare earth strontium aluminate, 0.04% of phosphite, 0.08% of antioxidant 1010 and 168 of antioxidant, 1% of KH-560 silane coupling agent; Carbonate and toughener A-612 accounting for 0.2% of the total mass of the luminous fiber.
[0042] The steps of the preparation method of the rare earth strontium aluminate long-lasting luminous fiber with skin-core structure in this embodiment are as follows:
[0043] (1) Preparation of PA6 luminous masterbatch: 68.8% of PA6 slices, 30% of rare earth strontium aluminate, 0.04% of phosphite, 0.08% of antioxidant 1010 and 168, and 1% of KH-560 silane coupling agent are used at high speed The mixer is mixed evenly, and then the...
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