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A method for preparing niobium monoxide and niobium powder mixture by plasma decomposition

A niobium monoxide and mixture technology is applied in the field of ion decomposition to prepare a mixture of niobium monoxide and niobium powder.

Active Publication Date: 2018-11-06
江西波德新材料研究有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the raw material niobium monoxide used in the niobium monoxide capacitor has a complicated extraction process before the present invention, and needs multiple processes such as agglomeration and reduction to produce
Due to the large potential market for niobium monoxide at this stage, the traditional extraction method takes a long time, high cost, low efficiency, and high price, which cannot promote market development

Method used

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  • A method for preparing niobium monoxide and niobium powder mixture by plasma decomposition

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Effect test

Embodiment 1

[0023] In the embodiment of the present invention, a method for preparing a mixture of niobium monoxide and niobium powder by plasma decomposition, using niobium pentoxide as a raw material, performing plasma pyrolysis on it to prepare a mixture of niobium monoxide and niobium powder, the specific preparation steps are: Inject niobium pentoxide into the plasma gun through a powder feeder, the powder feeding rate is 20g / min; the powder feeding gas is argon, and the flow rate is 0.65m 3 / h; the ion gas is argon, and the flow rate is 2.5m 3 / h; the mixture of niobium monoxide and niobium powder is obtained by decomposing at the same time the high temperature of the plasma flame changes the particle shape, and the decomposition power is 14.37kW; through the action of gravity, the mixture of niobium monoxide and niobium powder obtained by decomposition falls into a pure water circulation The cooling device of the system, at the same time, inject argon gas into the cooling device to...

Embodiment 2

[0026] In the embodiment of the present invention, a method for preparing a mixture of niobium monoxide and niobium powder by plasma decomposition, using niobium pentoxide as a raw material, performing plasma pyrolysis on it to prepare a mixture of niobium monoxide and niobium powder, the specific preparation steps are: Inject niobium pentoxide into the plasma gun through the powder feeder, the powder feeding volume is 15g / min; the powder feeding gas is argon, and the flow rate is 0.75m 3 / h; the ion gas is argon, and the flow rate is 2.2 m 3 / h; the mixture of niobium monoxide and niobium powder is obtained by decomposing at the same time the high temperature of the plasma flame changes the particle shape, and the decomposition power is 20kW; through the action of gravity, the mixture of niobium monoxide and niobium powder obtained by decomposition falls into the pure water circulation system At the same time, argon gas is injected into the cooling device to protect the produ...

Embodiment 3

[0029] In the embodiment of the present invention, a method for preparing a mixture of niobium monoxide and niobium powder by plasma decomposition, using niobium pentoxide as a raw material, performing plasma pyrolysis on it to prepare a mixture of niobium monoxide and niobium powder, the specific preparation steps are: Feed niobium pentoxide into the plasma gun through a powder feeder, the powder feeding volume is 22g / min; the powder feeding gas is argon, and the flow rate is 0.7m 3 / h; the ion gas is argon, the flow rate is 2.4m 3 / h, through the high temperature of the plasma flame to change the particle shape and decompose at the same time to obtain a mixture of niobium monoxide and niobium powder, the decomposition power is 15kW; through the action of gravity, the mixture of niobium monoxide and niobium powder obtained by decomposition falls into a pure water circulation system At the same time, argon gas is injected into the cooling device to protect the product from oxi...

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Abstract

Te invention discloses a method for preparing a niobium monoxide and niobium powder mixture through plasma decomposition. According to the method for preparing the niobium monoxide and niobium powder mixture through plasma decomposition, niobium pentoxide is used as a raw material, high-temperature plasma decomposition is conducted on the niobium pentoxide, and then the niobium monoxide and niobium powder mixture is prepared. The method for preparing the niobium monoxide and niobium powder mixture through plasma decomposition comprise the specific steps that the niobium pentoxide is poured into a plasma gun, the decomposition action is conducted through the high temperature of a plasma flame, and then the niobium monoxide and niobium powder mixture is obtained, wherein the power is controlled to be in the range of 10-100 kw; and the niobium monoxide and niobium powder mixture obtained through decomposition falls into a cooling device. The method for preparing the niobium monoxide and niobium powder mixture through plasma decomposition achieves simple and rapid reparation of the niobium monoxide and niobium powder mixture and is low in energy consumption and free of pollution. Besides, the particle shape of the obtained niobium monoxide and niobium powder mixture is sphere, the sphere particle shape is an ideal particle shape for manufacturing of a capacitor, and the niobium monoxide and niobium powder mixture is low in cost and good in quality. The method for preparing the niobium monoxide and niobium powder mixture through plasma decomposition has important significance in the aspects of replacing tantalum with niobium, replacing a tantalum capacitor and an aluminum capacitor with the niobium capacitor, manufacturing of a supercapacitor and the like.

Description

technical field [0001] The invention relates to a method for preparing a mixture of niobium monoxide and niobium powder, in particular to a method for preparing the mixture of niobium monoxide and niobium powder by plasma decomposition. Background technique [0002] At present, the main raw material of capacitors at home and abroad is mainly tantalum powder. However, the process of preparing tantalum powder is very complicated, and the tantalum element is usually stored in granite in nature, which is very difficult to extract, and the tantalum element that exists objectively in the world is very scarce. Considering all aspects, niobium is usually used instead of tantalum powder at home and abroad to solve the shortage of tantalum powder used in capacitors. [0003] In today's niobium-substituted tantalum articles, niobium powder or niobium monoxide is mostly used. Niobium monoxide can be used as a raw material to replace tantalum powder to make electrolytic capacitors. Wit...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B22F9/30
CPCB22F9/30B22F2999/00B22F2202/13
Inventor 江民德艾玉青江澜
Owner 江西波德新材料研究有限公司
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