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Working fluid system applicable to water-base drilling fluid filter cake removal before well cementing

A technology of water-based drilling fluid and working fluid, which is applied in the direction of drilling composition, chemical instruments and methods, etc., can solve the problems of high corrosion degree and corrosion rate, and achieve the effect of improving the removal

Active Publication Date: 2017-05-10
SOUTHWEST PETROLEUM UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] (3) The most commonly used weighting agent for water-based drilling fluid is BaSO 4 Mainly, some CaCO is added during reservoir drilling 3 , the acidic scavenging solution system can still effectively dissolve CaCO 3 , but under alkaline conditions, it has not been found that it can effectively remove BaSO 4 , CaCO 3 Scavenging liquid system for weighting agent filter cake;
[0008] (4) Although corrosion inhibitors are added to the existing acidic cleaning liquid system, the corrosion degree and corrosion rate of the casing (screen) under the condition of acidic treatment liquid are higher than those under the condition of alkaline

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Measure 400ml of water, and add solid phase corrosion main agent, solid phase corrosion auxiliary agent, gel breaker, surfactant, and clay stabilizer in sequence. In the solution, 0.2% of solid-phase corrosion main agent DTPA, 0.3% of EDTA-2Na, 0.1% of solid-phase corrosion auxiliary agent oxalic acid, 0.15% of gel breaker sodium persulfate, 0.5% of surfactant nonylphenol polyoxyethylene ether, Clay stabilizer KCl 3%, then add KOH to adjust the pH to 13, fully stir until the solid phase is completely dissolved, and obtain a filter cake removal working solution. Use it to remove drilling fluid filter cake, drilling fluid density: 1.30g / cm 3 ; Filter cake removal solution heating temperature: 60 ℃; filter cake removal solution shear soaking time: 30min.

Embodiment 2

[0027] Measure 400ml of water, and add solid phase corrosion main agent, solid phase corrosion auxiliary agent, gel breaker, surfactant, and clay stabilizer in sequence. In the solution, 0.4% of solid phase corrosion main agent DTPA, 0.6% of EDTA-2Na, 0.7% of solid phase corrosion auxiliary agent sodium gluconate, 0.15% of gel breaker potassium persulfate, 0.5% of surfactant nonylphenol polyoxyethylene ether %, clay stabilizer KCl 3%, and then add KOH to adjust the pH to 13, and fully stir until the solid phase is completely dissolved to obtain a filter cake removal working solution. Use it to remove drilling fluid filter cake, drilling fluid density: 1.35g / cm 3 ; Filter cake removal solution heating temperature: 70 ℃; filter cake removal solution shear soaking time: 20min.

Embodiment 3

[0029] Measure 400ml of water, and add solid phase corrosion main agent, solid phase corrosion auxiliary agent, gel breaker, surfactant, and clay stabilizer in sequence. In the solution, 0.9% of solid-phase corrosion main agent EDTA-2Na, 0.6% of solid-phase corrosion auxiliary agent oxalic acid, 0.25% of gel breaker sodium persulfate, 1.25% of surfactant nonylphenol polyoxyethylene ether, clay stabilizer KCl 3 %, then add NaOH to adjust the pH to 14, fully stir until the solid phase is completely dissolved, and obtain a filter cake removal working solution. Use it to remove drilling fluid filter cake, drilling fluid density: 1.20g / cm 3 ; Filter cake removal solution heating temperature: 75 ℃; filter cake removal solution shear soaking time: 30min.

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PUM

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Abstract

The invention discloses a working fluid system applicable to water-base drilling fluid filter cake removal before well cementing. The working fluid system is composed of the following components in percentage by mass: 0.5-1.5% of solid-phase denudation main agent, 0.1-1% of solid-phase denudation aid, 0.15-0.5% of viscosity breaker, 0.5-1.5% of surfactant, 1-3% of clay stabilizer and the balance of water. The pH value of the solution is regulated to 12-14 by NaOH or KOH. The solid-phase denudation main agent is composed of any one or mixture of ethylenediamine tetraacetic acid, disodium edetate, diethyltriamine pentaacetic acid and pentasodium amino trimethylene phosphonate; and the solid-phase denudation aid is composed of any one or mixture of sodium gluconate, oxalic acid and potassium sodium tartrate. By combining the characteristics of well cementing operation, the working fluid system can shorten the construction time, has higher reaction speed, achieves the goals of removing the filter cake and enhancing the cementing strength of the well-cementing interface, and thus, has broad market prospects.

Description

technical field [0001] The invention relates to a working fluid system suitable for removing water-based drilling fluid filter cake before cementing in the process of oil and gas exploration and development. Background technique [0002] During the drilling of oil and gas wells, the drilling fluid is filtered off under the action of differential pressure, and solid particles accumulate on the well wall to form a filter cake. Drilling fluid filter cake is an important factor to reduce the damage of drilling fluid to the reservoir, maintain the stability of the wellbore wall and the quality of the wellbore. However, since the drilling fluid filter cake itself has no consolidation ability and low strength, after cementing and cementing, the filter cake becomes a weak layer between the cement sheath and the well wall, which may form channeling channels in the later stage, resulting in formation fluids (oil, gas, water) channeling occurs. Therefore, in the process of circulatin...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/524C09K8/528
CPCC09K8/524C09K8/528C09K2208/12C09K2208/26
Inventor 黄盛郭小阳李早元张兴国刘亚鑫程小伟刘健李明辜涛刘开强
Owner SOUTHWEST PETROLEUM UNIV
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