A facile preparation method for low-cost high-strength repairable superhydrophobic coatings
A super-hydrophobic coating, high-strength technology, applied in coatings, epoxy resin coatings, etc., can solve the problems of high production cost of super-hydrophobic coating surface, complicated preparation or coating method, and difficult to prepare in large area. High mechanical strength, low cost and wide applicability
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Embodiment 1
[0032] (1) Preparation of epoxy resin superhydrophobic suspension coating: 1.67g of metal oxide powder MgO, 0.33g of metal oxide powder P25 and 2g of stearic acid as a low surface energy modifier were added to a solvent of 20mL of acetone. After stirring for 10 minutes, 1.2 g of epoxy resin (E51) and its curing agent were added to the system at a ratio of 3:1, and after ultrasonic treatment for 20 minutes, the stirring was continued to obtain an epoxy resin superhydrophobic suspension coating.
[0033] (2) Preparation of epoxy resin superhydrophobic coating: the epoxy resin superhydrophobic suspension coating obtained in step A was applied to the glass substrate by drop coating technique with a dropper. After curing and drying at 70°C for 5 hours, an epoxy superhydrophobic coating can be obtained on the glass substrate (see figure 1 ), the water droplets stand on its surface in a nearly perfect spherical shape. Its contact angle to water is 152°, and its rolling angle is abou...
Embodiment 2
[0036] (1) Preparation of epoxy resin superhydrophobic suspension coating: 1 g of metal oxide powder MgO, 1 g of metal oxide powder P25 and 2 g of stearic acid as a low surface energy modifier were added to 20 mL of acetone solvent. After stirring for 30 minutes, 1.2 g of epoxy resin (E51) and its curing agent were added to the system at a ratio of 3:1, and after ultrasonic treatment for 20 minutes, the stirring was continued to obtain an epoxy resin superhydrophobic suspension coating.
[0037] (2) Preparation of epoxy resin superhydrophobic coating: coating the epoxy resin superhydrophobic suspension obtained in step A, immersing the copper grid in the superhydrophobic suspension for a few seconds and slowly extracting it. After curing and drying at 70°C for 5 hours, an epoxy superhydrophobic coating can be obtained on the copper grid (see Figure 5 ), water droplets can also stand on its surface in a nearly perfect spherical shape.
Embodiment 3
[0039] (1) Preparation of epoxy resin superhydrophobic suspension coating: 1.67g of metal oxide powder MgO, 0.33g of metal oxide powder P25 and 2g of stearic acid as a low surface energy modifier were added to a solvent of 20mL of acetone. After stirring for 15 minutes, 1.2 g of epoxy resin (E51) and its curing agent were added to the system at a ratio of 3:1. After ultrasonic treatment for 60 minutes, the stirring was continued to obtain an epoxy resin superhydrophobic suspension coating.
[0040] (2) Preparation of epoxy resin superhydrophobic coating: the epoxy resin superhydrophobic suspension coating obtained in step A was applied to the glass substrate by drop coating technique with a dropper. After curing and drying at room temperature for 24 hours, an epoxy superhydrophobic coating can be obtained on the glass substrate.
[0041] (3) Repairable experiment: the obtained glass substrate with superhydrophobic coating is immersed in 1M sodium hydroxide solution for 30 seco...
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