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Method for preparing anti-sludge type concrete water reducing agent

A technology of concrete water reducer and anti-mud type, which is applied in the field of preparation of anti-mud type concrete water reducer, which can solve the problem of poor slump-preserving effect, lower water-reducing rate of polycarboxylate water-reducing agent, lower water-reducing rate, etc. problem, to achieve the effect of ensuring the compressive strength

Inactive Publication Date: 2017-05-31
衡阳市银利实业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

During the concrete mixing process, the polycarboxylate superplasticizer is partially absorbed by the clay, and the adsorbed superplasticizer loses its water-reducing function, so that the water-reducing rate of the polycarboxylate superplasticizer decreases. As the amount of mud increases, the adsorbed water reducing agent also increases, so the water reducing rate decreases with the increase of mud content in the aggregate, and the slump protection effect becomes worse.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment approach

[0011] As an embodiment of the present invention, a method for preparing a mud resistant concrete water reducer includes the following steps:

[0012] The first step is based on 9% maleic anhydride, 3.5% acrylic acid, 8.5% acrylamide, sodium dodecylbenzene sulfonate 7%, potassium permanganate 5.5%, sodium hydroxide 2%, water-soluble dextrin 3 %, propylene glycol methyl ether 4%, the balance is the weight ratio of water. Prepare each component and put it in the corresponding container. Take a part of the water from the container and add it to the reaction kettle. Heat the water to 80-90°C, then add maleic anhydride into the reaction kettle while stirring;

[0013] In the second step, after the maleic anhydride is stirred and mixed uniformly, sodium dodecylbenzene sulfonate, acrylic acid, and acrylamide are added to the reaction kettle in sequence;

[0014] The third step is to heat the solution to 90-95°C under airtight conditions for 1.5 hours;

[0015] In the third step, cool the so...

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PUM

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Abstract

The invention provides a method for preparing an anti-sludge type concrete water reducing agent. The method comprises the following steps: I, preparing the following components in percentage by weight: 9% of maleic anhydride, 3.5% of crylic acid, 8.5% of acrylic amide, 7% of sodium dodecyl benzene sulfonate, 5.5% of potassium permanganate, 2% of sodium hydroxide, 3% of water-soluble dextrin, 4% of propylene glycol monomethyl ether and the balance of water, adding a part of the water into a reaction kettle, heating to 80-90 DEG C, and adding the maleic anhydride; II, after the maleic anhydride is stirred and mixed uniformly, sequentially adding the sodium dodecyl benzene sulfonate, the crylic acid and the acrylic amide; III, heating the solution to 90-95 DEG C under a sealed condition, and keeping the temperature for 1.5 hours; III, cooling the solution to 40-45 DEG C, sequentially adding the propylene glycol monomethyl ether and the potassium permanganate, and continuously stirring for 30 minutes; IV, cooling the solution to 25-30 DEG C, sequentially adding the water-soluble dextrin, the sodium hydroxide and the water, and continuously stirring for 20 minutes, thereby obtaining the anti-sludge type concrete water reducing agent.

Description

Technical field [0001] The invention relates to the technical field of concrete admixtures, in particular to a method for preparing a mud-resistant concrete water reducer. Background technique [0002] Compared with naphthalene-based, aliphatic, sulfonated melamine and other water-reducing agents, the advantages of polycarboxylic acid-based water-reducing agents are: good slump retention; under the same fluidity, it has less impact on cement setting time, and can Effectively solve the problems of water reduction, air entrainment, retardation, bleeding, etc.; more slag or fly ash can be used to replace cement, thereby reducing the cost; no harmful substances such as formaldehyde, naphthalene, etc., will not cause environmental pollution, etc. At the same time, compared with other water-reducing agents, polycarboxylate water-reducing agents have higher requirements for the mud content of aggregates, and the water-reducing rate of polycarboxylate water-reducing agents decreases due ...

Claims

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Application Information

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IPC IPC(8): C08F222/06C08F220/56C08F220/06C04B24/26C04B103/30
Inventor 高翊杰何小雄高浚峰
Owner 衡阳市银利实业有限公司