A kind of molded laser holographic recording material and its preparation method
A laser holographic and recording material technology, applied in the field of molded laser holographic recording materials and their preparation, and composite materials for molded laser holographic recording, can solve problems such as plate sticking, drop points, and defects, and reduce surface energy and improve Good compatibility and wear resistance
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example Construction
[0043] Correspondingly, the method for preparing the molded laser holographic recording material in the present invention specifically includes the following steps:
[0044] ① Disperse polytetrafluoroethylene powder in the monomer solution, and use electron beam irradiation to initiate the graft polymerization of the monomer on the surface of the polytetrafluoroethylene powder. After the irradiation is completed, the grafted modified polytetrafluoroethylene is obtained by suction filtration, washing and drying. Vinyl fluoride powder; the mass fraction of the monomer solution is 4wt.% to 40wt.%, and the mass ratio of the polytetrafluoroethylene powder to the monomer is 1 / 0.5 to 1 / 3; the dose rate of the electron beam irradiation 4kGy / pass~30kGy / pass (because the sample can pass through the conveyor belt to the electron beam flow, the dose rate unit kGy / pass means the dose per single pass), and the radiation dose is 20kGy~90kGy;
[0045] ②Using electron beam to irradiate PTFE powder ...
Embodiment 1
[0055] The molded laser holographic recording material in this embodiment includes acrylic resin and radiation-grafted polyglycidyl methacrylate modified polytetrafluoroethylene micropowder, wherein the particles of the radiation-grafted modified polytetrafluoroethylene micropowder are The diameter is 0.2 microns, and the mass ratio to the acrylic resin is 1 / 20.
[0056] The molded laser holographic recording material is prepared according to the following steps:
[0057] ① Disperse polytetrafluoroethylene micropowder in 4wt.% glycidyl methacrylate aqueous solution, irradiate the mixed solution with electron beam, and after completion, suction filtration, washing and drying to obtain grafted modified polytetrafluoroethylene micropowder. The mass ratio of polytetrafluoroethylene powder and glycidyl methacrylate is 1 / 0.5, the irradiation dose rate is 4kGy / pass, and the irradiation dose is 20kGy.
[0058] ② Disperse the graft-modified polytetrafluoroethylene fine powder obtained in ste...
Embodiment 2
[0062] The molded laser holographic recording material in this embodiment includes acrylic resin and radiation grafted polyacrylic acid modified polytetrafluoroethylene powder, wherein the particle size of the radiation grafted modified polytetrafluoroethylene powder is 0.2 microns, and The mass ratio of acrylic resin is 3 / 100.
[0063] The molded laser holographic recording material is prepared according to the following steps:
[0064] ① Disperse polytetrafluoroethylene micropowder in a 12wt.% acrylic acid aqueous solution, irradiate the mixed solution with electron beam, and after completion, suction filtration, washing, and drying to obtain grafted modified polytetrafluoroethylene micropowder. The mass ratio of polytetrafluoroethylene powder to acrylic acid is 1 / 1, the irradiation dose rate is 20kGy / pass, and the irradiation dose is 60kGy.
[0065] ② Disperse the graft-modified polytetrafluoroethylene fine powder obtained in step ① in butyl acetate to obtain a graft-modified pol...
PUM
| Property | Measurement | Unit |
|---|---|---|
| particle diameter | aaaaa | aaaaa |
| particle diameter | aaaaa | aaaaa |
| particle diameter | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More - R&D
- Intellectual Property
- Life Sciences
- Materials
- Tech Scout
- Unparalleled Data Quality
- Higher Quality Content
- 60% Fewer Hallucinations
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2025 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com



