Anisotropic SmCo<5> type rare earth permanent magnet material and preparation method therefor
A kind of rare earth permanent magnet and anisotropic technology, which is applied in the direction of magnetic materials, inductor/transformer/magnet manufacturing, magnetic objects, etc., can solve the problems of small supercooling degree, low quenching speed, insufficient supercooling degree, etc., and achieve high Effects of residual magnetization, easy process control, and excellent magnetic properties
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Embodiment 1
[0051] SmCo will be stoichiometrically 4.95 C 0.05 Proportioning, wherein the weight of Sm is increased by 3wt% to make up for the Sm volatilized due to high vapor pressure during the smelting process. Put Sm, Co and graphite with a purity higher than 98% in the crucible of the melting furnace, and evacuate to make the vacuum degree reach 5×10 -2 Pa; pass high-purity argon to make the pressure in the melting furnace 50kPa, and melt it with electricity; and use electromagnetic force to automatically stir the liquid for refining. The temperature of the alloy liquid is 1200-1400 ° C, and keep it warm for 6 minutes; cast the evenly smelted alloy liquid Put it in a water-cooled copper mold for use; then, break the cooled alloy ingot into pieces and put it into a quartz tube with a diameter of 10mm in a vacuum stripping machine. The bottom of the quartz tube has a small hole with a diameter of about 0.5mm as a nozzle; Vacuumize the cavity of the vacuum belt throwing machine until ...
Embodiment 2
[0055] The stoichiometric ratio Sm(Co 0.99 Ti 0.01 ) 4.95 C 0.05 Proportioning, wherein the weight of Sm is increased by 8wt% to make up for the Sm volatilized due to high vapor pressure during the smelting process. Put Sm, Co, TiC and graphite with a purity higher than 98% in the crucible of the melting furnace, and evacuate to make the vacuum degree reach 1×10 -2 Pa; pass high-purity argon gas to make the pressure in the melting furnace 50kPa, and melt it with electricity; and use electromagnetic force to automatically stir the liquid for refining. The temperature of the alloy liquid is 1200-1400 ° C, and keep it warm for 4 minutes; cast the evenly smelted alloy liquid Put it in a water-cooled copper mold for use; then, break the cooled alloy ingot into pieces and put it into a quartz tube with a diameter of 10mm in a vacuum stripping machine. The bottom of the quartz tube has a small hole with a diameter of about 0.5mm as a nozzle; Vacuumize the cavity of the vacuum bel...
Embodiment 3
[0059] The stoichiometric ratio Sm(Co 0.7 Ti 0.3 ) 3 C 2 Proportioning, wherein the weight of Sm is increased by 5wt% to make up for the Sm volatilized due to high vapor pressure during the smelting process. Put Sm, Co, TiC and graphite with a purity higher than 98% in the crucible of the melting furnace, and evacuate to make the vacuum degree reach 1×10 -2 Pa; pass high-purity argon gas to make the pressure in the melting furnace 50kPa, and melt it with electricity; and use electromagnetic force to automatically stir the liquid for refining. The temperature of the alloy liquid is 1200-1400 ° C, and keep it warm for 4 minutes; cast the evenly smelted alloy liquid Put it into a water-cooled copper mold for use; then, crush the cooled alloy ingot and put it into a quartz tube with a diameter of 10 mm in a vacuum stripping machine. The bottom of the quartz tube has a small hole with a diameter of about 0.5 mm as a nozzle; Vacuumize the cavity of the vacuum belt throwing machi...
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