Cellulosic fiber containing kendir and preparation method thereof
A technology of cellulose fiber and apocynum, applied in the field of cellulose fiber and its preparation, can solve the problems of waste of resources, loss of functional components, waste of functional components, etc., and achieve the effects of good hygroscopicity, avoidance of loss and firm bonding
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Embodiment 1
[0047] Embodiment 1 A kind of preparation method of the cellulose fiber containing apocynum
[0048] Include the following steps:
[0049] (1) Preparation of modified functional component composite particles
[0050] Dissolve the extracts of Apocynum venetus, Herba Cortex and Radix Radix Radix in purified water to obtain a functional component solution with a mass concentration of 1.3mg / mL; add the functional component solution at a rate of 20mL / h with a mass concentration of 1.1mg In the chitosan acetic acid solution of / mL, control the stirring speed to be 350r / min, add quaternary ammonium starch ether, then filter, defoam after stirring evenly, obtain the chitosan acetic acid solution containing the functional component; Then with 7ml / min The speed is sprayed into the sodium hydroxide solution, granulated, and the modified functional component composite particles of 1-2 microns are generated.
[0051] The preparation method of described chitosan acetic acid solution, chit...
Embodiment 2
[0071] Embodiment 2 A kind of preparation method of the cellulose fiber containing apocynum
[0072] Include the following steps:
[0073] (1) Preparation of modified functional component composite particles
[0074] Dissolve the extracts of Apocynum venetus, Herba Cortex and Radix Radix Radix in purified water to obtain a functional component solution with a mass concentration of 1.5 mg / mL; add the functional component solution at a rate of 25 mL / h with a mass concentration of 1.5 mg In the chitosan acetic acid solution of / mL, control the stirring speed to be 450r / min, add quaternary ammonium starch ether, then filter, defoam after stirring evenly, obtain the chitosan acetic acid solution containing functional components; then with 9ml / min The speed is sprayed into the sodium hydroxide solution, granulated, and the modified functional component composite particles of 1-2 microns are generated.
[0075] The preparation method of described chitosan acetic acid solution, chit...
Embodiment 3
[0095] The synergistic effect of embodiment 3 functional components
[0096] On the basis of Example 1, only change the ratio of Apocynum apocynum extract, Grass coral extract, Radix Radix isatidis extract, mass parts, change see Table 1, the total amount of the extract of each test is 7 mass parts; measure Antibacterial effect of prepared fibers.
[0097] Table 1 Synergistic effect of functional ingredients
[0098]
[0099] It can be seen from Table 1 that the combination of isatidis extract, grass coral extract and apocynum extract has a synergistic effect on antibacterial.
[0100] Unless otherwise specified, the percentages used in the present invention are all weight percentages, and the ratios described in the present invention are all mass ratios.
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