Preparation method of mold release agent durable in storage
The technology of a release agent and fluorodecyltrimethoxysilane is applied in the field of preparation of a storage-resistant release agent, which can solve the problems of easy delamination, easy oxidation, poor stability, etc. The effect of heat resistance
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Embodiment 1
[0014] In a 2000L reactor, add 100Kg of full (17) fluorodecyl trimethoxysilane, 12Kg of methoxy polyethylene glycol methacrylate, 4Kg of poly-4-methyl-1-pentene, and methyl iso Butyl methanol 200Kg, hydroxypropyl methylcellulose phthalate 5Kg, 5,7-difluoro-2,3-dihydrobenzofuran 5Kg, N-tert-butoxycarbonyl-N(imidazole)- (4-Methylbenzenesulfonyl)-L-histidine 0.05Kg, stirred at a speed of 1200rpm for 1h to obtain a release agent product. Number M-1.
Embodiment 2
[0016] In a 2000L reactor, add 100Kg of full (17) fluorodecyltrimethoxysilane, 5Kg of methoxypolyethylene glycol methacrylate, 1Kg of poly-4-methyl-1-pentene, and methyl iso Butyl methanol 100Kg, hydroxypropyl methylcellulose phthalate 1Kg, 5,7-difluoro-2,3-dihydrobenzofuran 1Kg, N-tert-butoxycarbonyl-N (imidazole)- (4-Methylbenzenesulfonyl)-L-histidine 0.01Kg, stirred at a speed of 1200rpm for 0.5h to obtain a release agent product. Number M-2.
Embodiment 3
[0018] In a 2000L reactor, add 100Kg of full (17) fluorodecyl trimethoxysilane, 20Kg of methoxy polyethylene glycol methacrylate, 8Kg of poly-4-methyl-1-pentene, and methyl iso Butyl methanol 300Kg, hydroxypropyl methylcellulose phthalate 10Kg, 5,7-difluoro-2,3-dihydrobenzofuran 10Kg, N-tert-butoxycarbonyl-N (imidazole)- 0.1Kg of (4-methylbenzenesulfonyl)-L-histidine was stirred for 1.5h at a speed of 1200rpm to obtain a release agent product. Number M-3.
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