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Preparation method of glycyrrhiza sweetening and moistening essence for mouth stick

A technology of licorice and mouth sticks, which is applied in the fields of essential oils/spices, tobacco, applications, etc., can solve the problems of cigarette tip spices, filter sticks polluting the environment, and cigarette aroma loss, etc., and achieve good development and application prospects. Avoid loss and pyrolysis, increase the effect of sweetness

Active Publication Date: 2017-08-18
CHINA TOBACCO JIANGXI IND CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the reported inorganic materials used in filters, such as activated carbon, montmorillonite, medical stone, attapulgite, etc., will cause the loss of cigarette aroma while reducing coke and harm, and will bring many safety hazards
Many cigarettes use functional filter rods, among which activated carbon filter rods are the most widely used, which will bring uncomfortable carbon smell to the smoke and pollute the environment in the production of filter rods
However, there is no research on the use of licorice in the preparation of flavorings for cigarette tip sticks.

Method used

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  • Preparation method of glycyrrhiza sweetening and moistening essence for mouth stick
  • Preparation method of glycyrrhiza sweetening and moistening essence for mouth stick

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] The raw materials of licorice are graded according to the year water content and other indicators, and the licorice of the appropriate grade is selected, crushed to the size of rice grains, and screened and filtered with a 5-mesh sieve. After filtering, configure the licorice mixture according to the mass ratio of licorice: cellulase: polyphenol oxidase: peroxidase = 14:1:1:1. Take 1kg of licorice mixture, add 3Kg of cysteine ​​in 70% ethanol solution, wherein the mass fraction of cysteine ​​is 10%, stir evenly, and control the central temperature to 55°C for warm soaking for 4h. After the solution was filtered with suction, the filtrate was collected and concentrated. The filtrate was divided into 4 parts, and the ethanol was spin-dried at 60°C by a rotary evaporator to obtain an extract, and the ethanol was recovered for reuse. Add 350 mL of ethyl acetate to the extracted extract after spin-dried ethanol, and ultrasonically extract for 10 min. The extract was filter...

Embodiment 2

[0034] Glycyrrhizae raw material is pulverized and sieved in the manner of Example 1. After filtering, configure the licorice mixture according to the mass ratio of licorice: cellulase: polyphenol oxidase: peroxidase = 18:1:1:1. Take 1kg of licorice mixture, add 4Kg of cysteine ​​in 70% ethanol solution, wherein the mass fraction of cysteine ​​is 10%, stir evenly, and control the central temperature to 55°C for warm soaking for 4h. After the solution was filtered with suction, the filtrate was collected and concentrated. The filtrate was divided into 4 parts, and the ethanol was spin-dried at 60°C by a rotary evaporator to obtain an extract, and the ethanol was recovered for reuse. Add 350 mL of ethyl acetate to the extracted extract after spin-dried ethanol, and ultrasonically extract for 10 min. The extract was filtered with suction and the ethyl acetate contained therein was spin-dried until no liquid remained. Ethyl acetate was collected for reuse. Sweep the extract th...

Embodiment 3

[0036] Glycyrrhizae raw material is pulverized and filtered according to the manner of Example 1. After filtering, configure the licorice mixture according to the mass ratio of licorice: cellulase: polyphenol oxidase: peroxidase = 20:1:1:1. Take 1kg of licorice mixture, add 5Kg of cysteine ​​in 70% ethanol solution, wherein the mass fraction of cysteine ​​is 10%, stir evenly, and control the central temperature at 55°C for warm soaking for 4h. After the solution was filtered with suction, the filtrate was collected and concentrated. The filtrate was divided into 4 parts, and the ethanol was spin-dried at 60°C by a rotary evaporator to obtain an extract, and the ethanol was recovered for reuse. Add 350 mL of ethyl acetate to the extract after spin-dried ethanol, and extract by ultrasonic for 15 min. The extract was filtered with suction and the ethyl acetate contained therein was spin-dried until no liquid remained. Ethyl acetate was collected for reuse. Sweep the extract t...

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Abstract

The invention belongs to the technical field of tobacco flavors and in particular relates to a method of preparing essence of a mouth stick for a cigarette by taking glycyrrhiza as extract. The essence is used for improving sucking sweet feel of tobacco and enhancing the sensing comfort, so that the sucking quality of tobacco is effectively enhanced. The preparation method of glycyrrhiza sweetening and moistening essence for the mouth stick comprises the following steps: enzymolysis, alcohol extraction, extraction and the like. The prepared essence is directly added in a mouth stick processing step, so that escape and pyrolysis of essence in the storage and ignition and suction processes of tobacco are avoided, the loss of flavors in static igniting period of the tobacco can be also avoided, throttling of cut tobacco and filter tip on the flavors can be reduced, and the transfer efficiency is increased. The glycyrrhiza sweetening and moistening essence for the mouth stick prepared by the invention can remarkably improve the quality of fragrance of the cigarette, reduce the irritation and improve the quality of the cigarette.

Description

technical field [0001] The invention belongs to the technical field of flavorings for tobacco, and in particular relates to a method for preparing sweetening and moisturizing flavors for mouth sticks by using licorice as an extract. Background technique [0002] Glycyrrhiza licorice is the root or rhizome of the leguminous plant Glycyrrhizae licorice, which is a perennial herb. It is a traditional Chinese medicine commonly used in traditional Chinese medicine. Phlegm and cough medicine are used in combination to reduce the irritation to the mucous membrane of the oral cavity, relieve toxicity, and protect liver function. Bronchitis, pharyngitis, bronchial asthma, and chronic adrenal insufficiency also have a relieving effect. my country's licorice is mainly distributed in Xinjiang, Inner Mongolia, Gansu, Ningxia and other places, with rich resources, high reserves and excellent quality. Its chemical composition is complex, mainly containing several major compounds such as ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/02A24D3/02
CPCA24D3/0212C11B9/025
Inventor 邵灯寅胡巍耀何力李赓罗海涛田耀伟占小林任周营艾亦旻彭春鸣索卫国蔡继宝
Owner CHINA TOBACCO JIANGXI IND CO LTD
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