Alkali-containing high strain-point glass and preparation method thereof
A high-strain, glass technology, applied in glass manufacturing equipment, glass furnace equipment, glass production, etc., can solve the problems of high melting temperature and poor light transmission performance of glass, and achieve low melting temperature, high product added value, Use a wide range of effects
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[0033] A kind of preparation method of alkali-containing high strain point glass of the present invention, it comprises the following steps,
[0034] 1) First, according to the mass fraction of raw materials, accurately weigh 38.0-43.4% of quartz sand, 0.4-0.8% of boric acid, 0.3-0.6% of borax, 0.1-1.5% of silicon carbide, and 9.0-14.0% of gallium oxide, 10.0-13.0% lithium carbonate, 1.5-3.5% lithium nitrate, 2.1-3.5% sodium carbonate, 0.5-1.5% sodium chloride, 0.2-0.8% calcium carbonate, 1.5-2.5% calcium phosphate, 4.5 ~6.5% basic magnesium carbonate, 0.8~1.5% strontium carbonate, 0.3~4.5% beryllium oxide, 0.16~0.5% tin chloride, 13.0~17.5% cullet;
[0035] 2) Then, put the weighed raw materials into the mixer in turn, and mix until the uniformity is greater than 98% to form a batch;
[0036] 3) Then, add half of the batch material into the platinum crucible that has been heated to 1450°C; then, heat up to 1550-1600°C through 15-30min, and keep it warm for 30min, then add th...
Embodiment 1
[0046] 1) First, according to the mass fraction of raw materials, accurately weigh 41.5% of quartz sand, 0.67% of boric acid, 0.51% of borax, 0.8% of silicon carbide, 11.2% of gallium oxide, 10.0% of lithium carbonate, and 2.95% of nitric acid Lithium, 2.66% sodium carbonate, 0.67% sodium chloride, 0.32% calcium carbonate, 1.89% calcium phosphate, 5.14% basic magnesium carbonate, 1.01% strontium carbonate, 4.5% beryllium oxide, 0.19% Tin chloride, 15.99% cullet;
[0047] 2) Then, put the weighed raw materials into the mixer in turn, and mix until the uniformity is greater than 98% to form a batch;
[0048] 3) Then, add half of the batch material into the platinum crucible that has been heated to 1450°C; then, raise the temperature to 1600°C after 30 minutes and keep it warm for 30 minutes, then add the remaining batch materials into the platinum crucible, and heat it to 1600°C after 30 minutes ℃, after holding for 360 minutes, the temperature of the furnace was lowered from 1...
Embodiment 2
[0055] 1) First, according to the mass fraction of raw materials, accurately weigh 38% of quartz sand, 0.8% of boric acid, 0.3% of borax, 0.1% of silicon carbide, 14.0% of gallium oxide, 12.7% of lithium carbonate, and 3.5% of nitric acid Lithium, 2.1% sodium carbonate, 1.5% sodium chloride, 0.2% calcium carbonate, 2.5% calcium phosphate, 4.5% basic magnesium carbonate, 1.5% strontium carbonate, 0.3% beryllium oxide, 0.5% Tin chloride, 17.5% cullet;
[0056] 2) Then, put the weighed raw materials into the mixer in turn, and mix until the uniformity is greater than 98% to form a batch;
[0057] 3) Then, add half of the batch material into the platinum crucible that has been heated to 1450°C; then, heat up to 1550°C after 15 minutes and keep it warm for 30 minutes, then add the rest of the batch material into the platinum crucible, and heat it up to 1550°C through 15 minutes ℃, after holding for 240 minutes, the furnace temperature was lowered from 1550 ℃ to 1420 ℃ in 30 minute...
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