Preparation method of fireproof glue for fireproof glass
A technology of fireproof glass and fireproof glue, which is applied in chemical instruments and methods, glass/slag layered products, adhesives, etc., can solve the problems of a large number of microbubbles in the glass interlayer and poor apparent quality, and achieve low cost and long fireproof time , the effect of high transmittance
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Embodiment 1
[0023] A preparation method for fireproof glue for fireproof glass, comprising the following steps:
[0024] 1. Add hydrophilic nano core-shell structure organic-inorganic hybrid particles into deionized water, stir at high speed for 30 minutes, and the stirring speed is 1800r / min to obtain solution 1;
[0025] 2. Add sodium fluorosilicate, sodium metaaluminate, water-based bentonite, char-forming agent, ammonium polyphosphate, cross-linking agent, basic zinc carbonate, water-based rosin emulsion and polysiloxane emulsion to solution one in turn, at 100 Heating and stirring at -120°C for 40-60 minutes to obtain solution 2;
[0026] 3. Place the solution 2 in a vacuum environment for vacuum pressurization, the pressure is 10MPa, pressurize for 20min, and obtain the crude fireproof glue;
[0027] 4. Add a 50% aqueous solution of potassium hydroxide to the crude product of the fireproof glue, and slowly stir for 20 minutes under vacuum to obtain the finished product.
[0028] T...
Embodiment 2
[0036] A preparation method for fireproof glue for fireproof glass, comprising the following steps:
[0037] 1. Add hydrophilic nano core-shell structure organic-inorganic hybrid particles into deionized water, stir at high speed for 30 minutes, and the stirring speed is 1800r / min to obtain solution 1;
[0038] 2. Add sodium fluorosilicate, sodium metaaluminate, water-based bentonite, char-forming agent, ammonium polyphosphate, cross-linking agent, basic zinc carbonate, water-based rosin emulsion and polysiloxane emulsion to solution one in turn, at 120 Heating and stirring at ℃ for 60 min to obtain solution 2;
[0039] 3. Place the solution 2 in a vacuum environment for vacuum pressurization, the pressure is 20MPa, pressurize for 30min, and obtain the crude fireproof glue;
[0040] 4. Add a 50% potassium hydroxide aqueous solution to the crude product of the fireproof glue, and slowly stir for 30 minutes under vacuum conditions to obtain the finished product.
[0041] The f...
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