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Microchannel reactor

A technology of microchannel reactor and microchannel reaction, applied in chemical/physical/physical chemical reactors, chemical instruments and methods, chemical/physical/physical chemical processes, etc. The problem of large pressure drop and low conversion rate of raw materials can be solved, so as to achieve the effect of improving the conversion rate of raw materials, increasing the degree of turbulence, and uniform temperature

Inactive Publication Date: 2017-10-03
SINOPEC ENG +1
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The Chinese patent with the notification number CN202893334U discloses a microchannel reactor. The microchannel reactor adopts a titanium alloy plate structure, and each titanium alloy cooling cover plate is provided with a cooling chamber and a reaction chamber. The microchannel reactor has the ability to Withstand high pressure and corrosion resistance, the disadvantage is that the reactant stays in the reaction chamber for a short time and the production efficiency is low
The Chinese patent with the notification number CN203540513U discloses a microchannel reactor for the methanation process. The microreaction channel is fixed on the support plate in the middle of the reactor, so it is difficult to eliminate the stress caused by thermal expansion and contraction
The Chinese patent with the notification number CN102151531A discloses a microchannel reactor and its method for the complete methanation of syngas. The microreactor is arranged in parallel with several reaction channels and heat transfer channels alternately, and the pressure drop of the reactor is relatively large. Difficult to withstand high pressure
The Chinese patents whose notification numbers are CN204841617U and CN204816459U apply the microchannel reactor to the coal-to-SNG methanation process, and the target product has high selectivity. The disadvantage is that the residence time of the feed gas in this type of reactor is relatively short. low raw material conversion rate

Method used

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Embodiment 1

[0070] Such as figure 1 As shown, the microchannel reactor used in this embodiment includes a radial cylindrical sealed pressure-bearing shell 2, an air inlet pipe 18, an air outlet pipe 23 and a radial catalytic reaction zone. The upper part of the air intake pipe 18 is provided with an air inlet 1 , the lower part is provided with a first gas distributor 3 , and the lower part of the first gas distributor 3 is provided with a second gas distributor 17 . Between the radial catalytic reaction zone and the bottom surface of the casing 2, a thermal insulation material zone 12 composed of a thermal insulation blanket is arranged. The radial catalytic reaction zone includes a coaxial central cylinder 8, which is in sealing connection with the top sealing plate 4 and the bottom sealing plate 10. There is an annular gap 14 between the central cylinder 8 and the shell 2, and the annular gap 14 is connected to the air intake pipe 18. Fluid communication, the central cylinder 8 has a ...

Embodiment 2

[0075] Such as image 3 , Figure 4 As shown, the structural parameters such as the inner diameter of the reactor shell, the height of the catalytic reaction zone, and the number of microchannels in the reactor of this embodiment are exactly the same as those of the reactor in Embodiment 1. The difference from Embodiment 1 is that in this embodiment, the flow guide element 25 is replaced by a conical surface, and the conical surface is also fixed by a fixed shaft, and the size of the conical surface is the same as that of the cone. The microchannel reactor can also be used for methanation reactions. The process conditions adopted in Example 1 are the same, and the conversion rate of raw materials obtained is consistent with the implementation.

Embodiment 3

[0077] Such as Figure 5 , Figure 6 As shown, the structural parameters such as the inner diameter of the reactor shell, the height of the catalytic reaction zone, and the number of microchannels in the reactor of this embodiment are exactly the same as those of the reactor in Embodiment 1. The difference from Example 1 is that in this embodiment, the flow guide element is replaced by a cone with a hemispherical surface, and the hemispherical surface is also fixed by a fixed shaft. The diameter of the spherical surface is 3mm, and the distance between the two spherical surfaces is 5mm. Each flow guide assembly contains There are 38 hemispherical guide elements, and the hemispherical surfaces are uniformly concave and set in the direction of the central tube.

[0078] The reactor proposed in this embodiment is applied to the reaction of coal-based synthesis gas to light olefins (C 2 = -C 4 = ), the amount of active metal Fe loaded in the conical tube is 11.0g / m 2 . The ...

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Abstract

The invention discloses a microchannel reactor. The reactor comprises a cylindrical sealed pressure-bearing shell body (2), a gas inlet pipe (18), a gas outlet pipe (23) and an upside radial catalytic reaction zone, wherein the radial catalytic reaction zone comprises a plurality of radial micro-reaction channels (15) which are of radial arrangement, and flow guiding components (16) which are used for improving a fluid turbulence action are arranged in the radial micro-reaction channels (15). Compared with the prior art, the microchannel reactor provided by the invention is low in active metal consumption, low in bed layer pressure drop and high in raw material conversion ratio and is free of gas bias and short-circuit phenomena, overheated areas of a catalyst are avoided, and the service life of the reactor is prolonged.

Description

technical field [0001] The invention relates to a microchannel reactor. Background technique [0002] At present, there are mainly two types of fixed bed reactors, one is axial fixed bed reactor, and the other is radial fixed bed reactor. The axial fixed bed reactor is relatively easy to design and process, and the operation is simple, but there are problems such as large size of reactor equipment, large pressure drop in the bed layer, easy occurrence of local runaway temperature, slow heat transfer, low conversion rate, obvious amplification effect and reactor Problems with high material grades. The radial bed reactor has a large height-to-diameter ratio, a small bed pressure drop, and a short residence time of the reactants in the catalyst bed, but it is difficult to achieve uniform distribution of the reactants in the radial direction, and the production intensity of the unit catalyst bed is low. [0003] In order to overcome the problems of low heat transfer and mass t...

Claims

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Application Information

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IPC IPC(8): B01J19/00
CPCB01J19/0093B01J2219/00835
Inventor 张旭戴文松蒋荣兴
Owner SINOPEC ENG
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