Composite antibacterial cellulose preservation box and preparation method thereof
A compound antibacterial and cellulose technology, applied in botany equipment and methods, chemicals for biological control, animal repellent, etc., can solve the problems of high toxicity of antibacterial agents, unsafe use, toxic gases, etc.
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[0012] In order to achieve the above object, the present invention provides a preparation method of a composite antibacterial cellulose fresh-keeping box, comprising the following steps: (1) pulverizing wormwood, Patrinia, Sophora sophora and Daqing, soaking in ethanol solution, Filtrate to obtain filtrate M1; (2) mix agarose with sodium carbonate and water, then add glacial acetic acid to react to obtain M2; (3) mix M1, M2, ferrous compound, reducing agent, methylisothiazole Mix ketone and surfactant to obtain M3; (4) Coat M3 on the inner wall of the cellulose fresh-keeping box and dry it.
[0013] In the above technical scheme, wormwood, Patrinia, bitter beans and Daqing can be fresh finished products, or dried wormwood, Patrinia, bitter beans and Daqing, in order to facilitate the preservation of raw materials in daily industrial production , preferably, the wormwood, Patrinia, Sophora and Daqing are all dried wormwood, Patrinia, Sophora and Daqing, and the moisture content...
Embodiment 1
[0035] The preparation of the composite antibacterial cellulose fresh-keeping box comprises the following steps:
[0036] (1) In parts by weight, crush 8 parts of wormwood, 2 parts of Patrinia, 6 parts of Sophora sophora, and 4 parts of Daqing until the average particle diameter is less than 0.5mm, and put them in 40 parts of 60% ethanol aqueous solution by volume Soak at 50°C for 12h, filter to obtain filtrate M1;
[0037] (2) In parts by weight, mix 20 parts of agarose, 3 parts of sodium carbonate and 40 parts of water, then add 5 parts of glacial acetic acid and react for 20 minutes to obtain M2;
[0038] (3) In parts by weight, 22 parts of M1, 8 parts of M2, 0.01 part of ferrous gluconate, 0.1 part of ascorbic acid, 1 part of methylisothiazolinone, 2 parts of dodecyldimethylbenzyl ammonium chloride Parts were mixed at 62°C for 30 minutes to obtain M3;
[0039] (4) Coat M3 on the inner wall of the cellulose fresh-keeping box at 100°C, and the coating amount of M3 is 9g / m ...
Embodiment 2
[0041] The preparation of the composite antibacterial cellulose fresh-keeping box comprises the following steps:
[0042] (1) In parts by weight, 12 parts of wormwood, 4 parts of Patrinia, 8 parts of Sophora sophorae, and 6 parts of Daqing are pulverized to an average particle size of less than 0.5mm, and they are mixed in 60 parts of 75% ethanol aqueous solution by volume Soak at 60°C for 36 hours, filter to obtain filtrate M1;
[0043] (2) In parts by weight, mix 30 parts of agarose, 5 parts of sodium carbonate, and 50 parts of water, then add 7 parts of glacial acetic acid and react for 40 minutes to obtain M2;
[0044] (3) In parts by weight, 32 parts of M1, 15 parts of M2, 0.03 part of ferrous gluconate, 0.2 part of ascorbic acid, 2 parts of methylisothiazolinone, 3 parts of dodecyldimethylbenzyl ammonium chloride Parts were mixed at 82°C for 45 minutes to obtain M3;
[0045] (4) Coat M3 on the inner wall of the cellulose fresh-keeping box at 120°C, and the coating amou...
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