Genome object region sequencing hybrid capture method
A technology of target region capture and hybrid capture, which is applied in the field of hybrid capture for genome target region sequencing, can solve the problems affecting the sequencing process, affecting the salt ion concentration of the mixed solution, and different operating conditions, so as to improve the capture efficiency and shorten the experiment time , the effect of moderate incubation time
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Embodiment 1
[0049] Embodiment 1 reagent preparation and storage
[0050] The water used for the preparation of the following reagents is nucleic acid-free water, and the containers used must be treated with nuclease before use.
[0051] 1) Note #1
[0052] 4*SSPE (ivitrogen, 15591043), packed in 1.5ml tubes, stored at 4 degrees.
[0053] 2) Note #2
[0054] 0.1M EDTA, pH 8.0 (ivitrogen, 15575020), aliquoted in 1.5ml tubes, stored at 4 degrees.
[0055] 3) Note#3
[0056] 50*denharts (invitrogen, 750018), packed in 1.5ml tubes, stored at -20 degrees.
[0057] 4) Note #4
[0058] 0.1% SDS (invitrogen, 15553027), diluted to 1 ×, distributed in 1.5ml tubes, stored at 4 degrees.
[0059] 5) Binding buffer:
[0060] Composition: NaCl, Tris-HCl, EDTA, pH7.5
[0061] Preparation:
[0062]
[0063] 6) Wash Buffer 1 (Wash Buffer 1):
[0064]Composition: SSC, SDS
[0065] Preparation:
[0066]
[0067] 7) Wash Buffer 2 (Wash Buffer 2):
[0068] Composition: SSC, SDS
[0069] Prep...
Embodiment 2
[0079] Example 2 Design and customization of panel
[0080] 1. Generation of target area list
[0081] a) According to the design of the experiment, select the region to be sequenced, and use hg19 as the reference genome to establish a list of target regions, including chromosome numbers and starting point locations;
[0082] b) Target region adjustment: If the target region is less than 220bp, extend to both ends to 220bp.
[0083] 2. Assess the GC content of the target region
[0084] For regions with a GC content higher than 70% or lower than 30%, design 1× to 2× tiling probes.
[0085] 3. Probe Generation
[0086] a) Generate a probe group with a length of 110bp in the form of a tile array (tiling array), that is, regularly intercept the sequence of the genome according to a certain degree of overlap as the probe sequence (such as 2 × tiling design, the interval length is 55bp; 3 ×tiling design, interval length is 37bp);
[0087] b) For regions with a GC content highe...
Embodiment 3
[0100] The preparation of embodiment 3 probe
[0101] This example introduces the preparation and storage of probes. The consumables required for the experiments in this chapter must be non-nucleic acid consumables. Gloves and masks should be worn throughout the process, and the operation should be performed on a clean bench.
[0102] 1. Probe template preparation
[0103] 1) First take 5 μl of the probe stock solution, dilute it to 3ng / μl with 10mM Tris-HCl buffer, aliquot 4.2μl / tube, take one tube and continue with the following steps, and freeze the rest at -80°C;
[0104] 2) According to the following system and procedures, do 2 tubes in parallel;
[0105] reaction system:
[0106] KAPA HIFI library amplification Kit
25μl
Rev (25μM)
1μl
SP6promoter (25μM)
1μl
1μl
water
22μl
[0107] Reaction procedure:
[0108]
[0109] 3) Qubit quantification: Take 1 μl of PCR product for qub...
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