Fructus gardeniae facial mask powder and preparation method thereof

A technology of gardenia mask and mask powder, which is applied in the field of gardenia mask powder and its preparation, to achieve the effects of improving metabolism, alleviating aging, and inhibiting abnormal keratinization process

Active Publication Date: 2017-12-01

宁德市容海水产有限公司

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AI-Extracted Technical Summary

Problems solved by technology

[0004] There are fewer facial masks specifically for the effi...

Abstract

The invention provides fructus gardeniae facial mask powder and a preparation method thereof. The facial mask powder consists of the following raw materials in parts by weight: 25-35 parts of fructus gardeniae iridoid glycoside powder, 5-10 parts of rhododendron simsii planch, 1-5 parts of a gardenia florida extract, 5-15 parts of a camellia sinensis leaf extract, 20-23 parts of konjac gum, 12-16 parts of seaweed gel and 10-16 parts of collagen. The facial mask provided by the invention contains fructus gardeniae iridoid glycoside substances, and since camellia sinensis leaf, konjac gum and seaweed gel are pure herbal ingredients, the facial mask is free from preservatives and additives and is free from skin irritation or hurt; fragrance of the camellia sinensis leaf is reserved; and the facial mask can take a relatively good curative effect on cystic acne formed by festering of whelk.

Application Domain

Cosmetic preparationsToilet preparations +3

Technology Topic

Camellia sinensisGardenia jasminoides +12

Examples

Experimental program(3)
Effect test(1)

Example Embodiment

[0026] Example 1

[0027] A gardenia facial mask powder, comprising the following raw materials in parts by weight: 30 parts of gardenia iridoid glycoside powder, 8 parts of azalea extract, 3 parts of gardenia flower extract, 10 parts of white tea extract, 22 parts of konjac gum, 14 parts of seaweed gum and 13 parts of collagen.

[0028] The method for preparing the gardenia iridoid glycoside powder is:

[0029] (1) Freeze-drying: select high-quality gardenias and gardenias, soak the gardenias and gardenias in 0.1wt.% food-grade hydrogen peroxide solution respectively, soak for 5 minutes, rinse with water and drain the water. The pre-treated gardenias and gardenias were freeze-dried in a vacuum freeze dryer, and the moisture content of the gardenias and gardenias after freeze-drying was 8%;

[0030] (2) Breaking the shell: breaking the gardenia shell, removing the gardenia shell;

[0031] (3) Degreasing treatment: Take the broken gardenia, smash it through a 15-mesh sieve, and place it in a carbon dioxide supercritical extraction kettle for deoiling. The carbon dioxide supercritical extraction parameters are: extraction pressure 28MPa, extraction preheating The device temperature is set at 43℃, the carbon dioxide flow rate is 700L/H, the separation pressure is 10MPa, the separation temperature is 53℃, and the separation time is 2 hours. The crude fat content of the deoiled gardenia is less than 1.0%;

[0032] (4) Superfine pulverization: the defatted gardenia and freeze-dried gardenia by supercritical carbon dioxide extraction are superfinely pulverized to 400 meshes to obtain gardenia powder;

[0033] (5) Iridoid glycoside extraction: The solid-liquid mass ratio of gardenia powder and edible ethanol is 1:7, the microwave power is 1000w, the extraction temperature is 45℃, and the extraction is 50min;

[0034] (6) Clarification and filtration treatment: the microwave-extracted solution is centrifuged and filtered, the supernatant is taken, and the final concentration is pectinase 0.06%, chitosan 0.03% and honey 1.0% for compound clarification. The temperature is 45℃ for 3 hours and filter;

[0035] (7) Concentration: take the supernatant from step (6) and concentrate it under a vacuum of 100 kPa and a temperature of 52°C with a density of 1.2 to obtain an iridoid glycoside concentrate paste;

[0036] (8) Freeze-drying: Iridoid glycoside concentrate paste is freeze-dried under vacuum pressure 80Pa, temperature -45℃, 25h, and the water content of iridoid glycoside extract is 1%, to prepare gardenia iridoid glycoside powder. The extraction rate is 85%.

Example Embodiment

[0037] Example 2

[0038] A gardenia facial mask, comprising the following raw materials in parts by weight: 25 parts of gardenia iridoid glycoside powder, 5 parts of azalea extract freeze-dried powder, 1 part of gardenia flower extract, 5 parts of white tea extract, and 20 parts of konjac gum Parts, 12 parts of seaweed gum, 10 parts of collagen.

[0039] The method for preparing the gardenia iridoid glycoside powder is:

[0040] (1) Freeze-drying: select high-quality gardenias and gardenias, soak the gardenias and gardenias in 0.1wt.% food-grade hydrogen peroxide solution respectively, soak for 4 minutes, rinse with clean water and drain the water , The pre-treated gardenias and gardenias are respectively freeze-dried in a vacuum freeze dryer, and the moisture content of the gardenias and gardenias after freeze-drying is required to be below 10%;

[0041] (2) Breaking the shell: breaking the gardenia shell, removing the gardenia shell;

[0042] (3) Degreasing treatment: Take the broken gardenias, smash them through a 10-mesh sieve, and put them in a carbon dioxide supercritical extraction kettle for deoiling. The carbon dioxide supercritical extraction parameters are: extraction pressure 25MPa, extraction preheating The temperature of the device is set at 40℃, the carbon dioxide flow rate is 600L/H, the separation pressure is 10MPa, the separation temperature is 50℃, and the separation time is 2 hours. The crude fat content of the deoiled gardenia is less than 1.0%;

[0043] (4) Superfine pulverization: The defatted gardenia by carbon dioxide supercritical extraction and the freeze-dried gardenia are superfinely pulverized to 350 mesh to obtain gardenia powder;

[0044] (5) Iridoid glycoside extraction: the solid-liquid mass ratio of gardenia powder and edible ethanol is 1:5, the microwave power is 500w, the extraction temperature is 40℃, and the extraction is 40min;

[0045] (6) Clarification and filtration treatment: the microwave-extracted solution is centrifuged and filtered, the supernatant is taken, and the final concentration of pectinase 0.8%, chitosan 0.04% and honey 1.5% are added for compound clarification. The temperature is 40℃ for 3h and filter;

[0046] (7) Concentration: take the supernatant of step (6) and concentrate it at a vacuum of 100 kPa and a temperature of 50°C with a density of 1.3 to obtain an iridoid glycoside concentrate paste;

[0047] (8) Freeze-drying: Iridoid glycoside concentrate paste is freeze-dried under vacuum pressure 50Pa, temperature -45℃, 25h, and the water content of iridoid glycoside extract is 1%, to prepare gardenia iridoid glycoside powder. The extraction rate is 75%.

Example Embodiment

[0048] Example 3

[0049] A gardenia facial mask, comprising the following raw materials in parts by weight: 35 parts of gardenia iridoid glycoside powder, 10 parts of azalea extract freeze-dried powder, 5 parts of gardenia flower extract, 15 parts of white tea extract, and 23 parts of konjac gum Parts, 16 parts of seaweed gum, 16 parts of collagen.

[0050] The method for preparing the gardenia iridoid glycoside powder is:

[0051] (1) Freeze-drying: select high-quality gardenias and gardenias, soak the gardenias and gardenias in 0.1wt.% food-grade hydrogen peroxide solution respectively, soak for 6 minutes, rinse with water and drain the water. The pre-treated gardenias and gardenias are respectively freeze-dried in a vacuum freeze dryer, and the moisture content of the gardenias and gardenias after freeze-drying is required to be below 10%;

[0052] (2) Breaking the shell: breaking the gardenia shell, removing the gardenia shell;

[0053] (3) Degreasing treatment: Take the broken gardenia, smash it through an 18-mesh sieve, and put it in a carbon dioxide supercritical extraction kettle for deoiling. The carbon dioxide supercritical extraction parameters are: extraction pressure 30MPa, extraction preheating The device temperature is set at 45℃, the carbon dioxide flow rate is 800L/H, the separation pressure is 10MPa, the separation temperature is 55℃, and the separation time is 2 hours. The crude fat content of the deoiled gardenia is less than 1.0%;

[0054] (4) Superfine pulverization: The defatted gardenia by carbon dioxide supercritical extraction and the freeze-dried gardenia are superfinely pulverized to 500 meshes to obtain gardenia powder;

[0055] (5) Iridoid glycoside extraction: The solid-liquid mass ratio of gardenia powder and edible ethanol is 1:8, the microwave power is 2000w, the extraction temperature is 50℃, and the extraction is 60min;

[0056] (6) Clarification and filtration treatment: the microwave-extracted solution is centrifuged and filtered, the supernatant is taken, and the final concentration is pectinase 0.1%, chitosan 0.05% and honey 2.0% for compound clarification, and the temperature is 50℃ for 3h and filter;

[0057] (7) Concentration: take the supernatant of step (6) and concentrate it under a vacuum of 100 kPa, a temperature of 55°C, and a density of 1.5 to obtain an iridoid glycoside concentrate paste;

[0058] (8) Freeze-drying: Iridoid glycoside concentrate paste is freeze-dried under vacuum pressure 100Pa, temperature -45℃, 25h, and the water content of iridoid glycoside extract is 1% to prepare gardenia iridoid glycoside powder. The extraction rate is 80%.

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Classification and recommendation of technical efficacy words

Significant effect
Regulate oil secretion

Fructus gardeniae facial mask powder and preparation method thereof

A technology of gardenia mask and mask powder, which is applied in the field of gardenia mask powder and its preparation, to achieve the effects of improving metabolism, alleviating aging, and inhibiting abnormal keratinization process

AI-Extracted Technical Summary

Problems solved by technology

Abstract

Examples

Example Embodiment

Example Embodiment

Example Embodiment

PUM

Description & Claims & Application Information

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