Method for preparing nanocarbon conductive fiber yttrium-niobium-aluminum superconducting material
A nano-carbon fiber and conductive fiber technology, applied in the usage of superconductor elements, superconducting devices, superconducting/high-conducting conductors, etc., can solve the problems of complex and difficult yttrium niobium aluminum superconducting materials and high equipment requirements, and achieve super The effect of good conductivity, good connectivity and high critical transition temperature
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Embodiment 1
[0019] Graphite pretreatment, adding sodium fluoride to the nano-graphite powder, adding a metal catalyst, mixing, heating at 600°C under the protection of an inert gas, and controlling the heating time to 10min, fixing sodium fluoride on the surface of the nano-graphite powder .
[0020] Nano-carbon fiber pretreatment, the nano-carbon fiber is oxidized with concentrated sulfuric acid and potassium permanganate mixed acid, after ultrasonic vigorous stirring, the carboxylated nano-carbon fiber is obtained, the surface treatment agent is added, heat treatment at 150 ° C for 10 minutes, and silver is added. Under the protection of a mixed gas of nitrogen and helium, heat at 400° C. for 30-45 minutes to uniformly disperse the silver in the carbon nanofibers.
[0021] Put pretreated graphite and pretreated nano-carbon fiber in a container, dissolve with 150 parts of isopropanol, then add dispersant, polyphenylene sulfide, PPS resin, blend with a strong mixer, and then use an ultras...
Embodiment 2
[0029] Graphite pretreatment, adding sodium fluoride to the nano-graphite powder, adding a metal catalyst, mixing, heating at 650°C under the protection of an inert gas, and controlling the heating time for 15 minutes, and fixing sodium fluoride on the surface of the nano-graphite powder .
[0030] Nano-carbon fiber pretreatment, the nano-carbon fiber is oxidized with concentrated sulfuric acid and potassium permanganate mixed acid, after ultrasonic vigorous stirring, to obtain carboxylated nano-carbon fiber, add surface treatment agent, heat treatment at 200 ° C for 15 minutes, add silver, in Under the protection of a mixed gas of nitrogen and helium, heat at 450° C. for 45 minutes to uniformly disperse the silver in the carbon nanofibers.
[0031] Put pretreated graphite and pretreated nano-carbon fiber in a container, dissolve with 250 parts of isopropanol, then add dispersant, polyphenylene sulfide, PPS resin, blend with a strong mixer, and then use an ultrasonic disperser...
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