The invention discloses a preparation method of a YBa2Cu3O7-
delta superconducting material, and relates to a preparation method of a superconductor material, which comprises the following steps: dissolving Y2 (CO3) 3, Ba (NO3) 2 and CuSO4. 5H2O in deionized water according to a
molar ratio, uniformly stirring, firstly adding
citric acid, then adding
ethylene glycol, then adding
ammonia water to adjust the pH value, carrying out
microwave heating and stirring to form
sol, carrying out
vacuum drying, and
grinding into particles, thereby obtaining the YBa2Cu3O7-
delta superconducting material. Carrying out gradient
sintering in an
oxygen atmosphere, and continuously carrying out
microwave treatment in the
sintering process; and carrying out gradient cooling in an
oxygen atmosphere, and carrying out ball milling, screening and
drying after cooling. According to the process method, the
microwave-assisted low-temperature
calcination technology and the
sol combustion method are combined,
energy consumption is remarkably reduced, the preparation period is obviously shortened,
material element distribution is more uniform, the superconductive critical temperature Tc is larger than or equal to 72K, the technical problems that a traditional process is high in high-temperature
energy consumption and uneven in component are solved, and the method can be applied to the fields of superconductive power grids,
quantum devices and the like on a large scale.