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Graphene air purification material and preparation method thereof

A graphene and air-purifying technology, applied in chemical instruments and methods, separation methods, and other chemical processes, can solve problems such as poor practicability, high cost, and difficulty in meeting the use of ultraviolet light strips, and achieve low production costs, Increased specific surface area, optimization and adsorption of pollutant gases, and effects of air purification

Active Publication Date: 2018-02-09
厦门信果石墨烯科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, since this type of photocatalysis can only work under the irradiation of ultraviolet light, the materials made in this way are not very practical at present, and the indoor environment is difficult to meet the use of ultraviolet light strips, and the cost is high

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] Take 100g of wood charcoal and crush it to 8-12μm; dissolve 50g of sodium hydroxide in 50mL of water, mix it evenly with the wood charcoal, and dry it under vacuum; The temperature was raised to 780°C and kept for 2 hours; after cooling to room temperature, the activated product was washed to neutrality, then 6M hydrochloric acid was added to reflux for 2 hours, and then washed with deionized water to neutrality; 4g of calcium carbonate whiskers, 300mL of 0.6wt% concentration of graphene aqueous dispersion, and 2 g of melamine was added to it, ultrasonically stirred for 1 h, and then spray-dried; the above material was placed in a reduction furnace, and the temperature was raised to 800 ° C at a rate of 10 ° C / min under the protection of hydrogen and kept for 2 h ; After the temperature drops to room temperature, the graphene super-purifying air composite material is obtained.

Embodiment 2

[0029] Take 100g of wood charcoal and crush it to 8-12um; dissolve 100g of sodium hydroxide in 100mL of water, mix it evenly with the wood charcoal, and dry it under vacuum; The temperature was raised to 780°C and kept for 2 hours; after cooling to room temperature, the activated product was washed to neutrality, then 6M hydrochloric acid was added to reflux for 2 hours, and then washed with deionized water to neutrality; 4g of calcium carbonate whiskers, 300mL of 0.6wt% concentration of graphene aqueous dispersion, and 2 g of melamine was added to it, ultrasonically stirred for 1 h, and then spray-dried; the above material was placed in a reduction furnace, and the temperature was raised to 800 ° C at a rate of 10 ° C / min under the protection of hydrogen and kept for 2 h After the temperature drops to room temperature, the graphene super-purifying air composite material is obtained.

Embodiment 3

[0031] Take 100g of wood charcoal and crush it to 8-12μm; dissolve 50g of potassium hydroxide in 50mL of water, mix it evenly with the wood charcoal, and dry it under vacuum; The temperature was raised to 780°C and kept for 2 hours; after cooling to room temperature, the activated product was washed to neutrality, then 6M hydrochloric acid was added to reflux for 2 hours, and then washed with deionized water to neutrality; 4g of calcium carbonate whiskers, 300mL of 0.6wt% concentration of graphene aqueous dispersion, and 2 g of melamine was added to it, ultrasonically stirred for 1 h, and then spray-dried; the above material was placed in a reduction furnace, and the temperature was raised to 800 ° C at a rate of 10 ° C / min under the protection of hydrogen and kept for 2 h ; After the temperature drops to room temperature, the graphene super-purifying air composite material is obtained.

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Abstract

The invention belongs to the field of air purification materials and particularly relates to a graphene air purification material and a preparation method thereof. The preparation method comprises steps as follows: A), wooden activated carbon powder activated by water vapor is mixed with alkali, and a semi-finished activated carbon product is obtained after a mixture is activated; B), the semi-finished activated carbon product obtained in the step A) is mixed with calcium carbonate whiskers, a nitrogen source and a graphene solution, a mixture is subjected to a reduction reaction, and the graphene air super-purification composite material is obtained. The material has the functions of adsorbing harmful gas and peculiar smell, inhibiting bacteria and killing bacteria and has the advantagesof being low in material production cost and free of pollution.

Description

technical field [0001] The invention belongs to the field of air purification materials, in particular to a graphene air purification material and a preparation method thereof. Background technique [0002] In recent years, the problem of air pollution has been an urgent problem for governments around the world. The flue gas released by burning fossil fuels (coal, oil, natural gas, etc.) in energy, chemical, metallurgy, transportation and other industries contains a large amount of SO 2 and NO x , causing serious air pollution. In addition, all kinds of dust produced by human activities, as well as the pollution of solid suspended particles such as sand and dust caused by climate deterioration, and the volatile organic pollutants from various decorative materials and oral chemicals are increasing. land into residential and public buildings, leading to a sharp increase in the degree of pollution of the living environment. [0003] According to the survey, 90% of newly ins...

Claims

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Application Information

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IPC IPC(8): B01J20/20B01J20/30B01D53/02
CPCB01D53/02B01J20/20
Inventor 刘乐光
Owner 厦门信果石墨烯科技有限公司