Preparation method of water-diverting coating fiber
A coating fiber and technology of preparation steps, which are applied in the field of preparation of water-conducting coating fibers, can solve problems such as small wet capacity, poor moisture release performance, and poor film-forming property, and achieve increased pore size, improved water-conducting performance, and improved Effect of Pore Size Distribution
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example 1
[0021] Take palm silk and mix it with glacial acetic acid according to the mass ratio of 1:5, heat it in a water bath at 55°C for 3h, filter to obtain the filter residue, wash it with deionized water for 3 times, and then dry it at 75°C for 6h to obtain Dry palm silk, by weight, weigh 45 parts of deionized water, 1 part of tetrapropylammonium bromide, 3 parts of tetrapropylammonium bromide, 3 parts of ethyl tetrasilicate and 3 parts of sodium oxide, stir and mix for 10 minutes, and use 10% hydrogen Sodium oxide solution adjusted the pH to 8.5, stirred and mixed to obtain the modified solution; according to the mass ratio of 1:10, dry palm fiber was added to the modified solution, stirred and mixed, and placed in a 185°C reactor for crystallization treatment for 18 hours, filtered to obtain The filter cake was washed 3 times with deionized water, and then dried at 75°C for 6 hours to obtain dry modified fibers, and then the dried modified fibers were placed in a tube-type atmosp...
example 2
[0023] Take palm silk and mix it with glacial acetic acid according to the mass ratio of 1:5, heat it in a water bath at 57°C for 4 hours, filter to obtain the filter residue, wash it with deionized water for 4 times, and then dry it at 77°C for 7 hours to obtain Dried palm fiber, weighed 47 parts of deionized water, 4 parts of tetrapropylammonium bromide, 4 parts of tetrapropylammonium bromide, 4 parts of tetrapropylammonium bromide, and 4 parts of sodium oxide were stirred and mixed for 12 minutes, and oxidized with a mass fraction of 10% Adjust the pH to 8.5 with sodium solution, stir and mix to obtain a modified solution; add dry palm fiber to the modified solution at a mass ratio of 1:10, stir and mix, and place in a reaction kettle at 187°C for crystallization treatment for 19 hours, and filter to obtain a modified solution. The cake was washed 4 times with deionized water, and then dried at 77°C for 7 hours to obtain dry modified fibers, and then the dried modified fiber...
example 3
[0025] Take palm silk and mix it with glacial acetic acid according to the mass ratio of 1:5, heat it in a water bath at 60°C for 5 hours, filter to obtain the filter residue, wash it with deionized water for 5 times, and then dry it at 80°C for 8 hours to obtain Dry palm silk, by weight, weigh 50 parts of deionized water, 2 parts of tetrapropylammonium bromide, 5 parts of tetrapropyl ammonium bromide, 5 parts of ethyl tetrasilicate and 5 parts of sodium oxide, stir and mix for 15 minutes, and use 10% hydrogen Sodium oxide solution adjusted the pH to 8.5, stirred and mixed to obtain the modified solution; according to the mass ratio of 1:10, dry palm fiber was added to the modified solution, stirred and mixed, and placed in a 190°C reactor for crystallization treatment for 20h, filtered to obtain The filter cake was washed 5 times with deionized water, and then dried at 85°C for 8 hours to obtain dry modified fibers, and then the dried modified fibers were placed in a tube-type...
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