Preparation method of porous vanadium-chromium-titanium material
A vanadium-chromium-titanium and mixing technology, which is applied in the field of powder metallurgy, can solve the problems of high cost, complex process, and low efficiency, and achieve the effect of low cost, simple production process, and uniform structure
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[0015] A preparation method of a porous vanadium-chromium-titanium material, comprising the following steps:
[0016] a, mixing materials, putting metal titanium powder, chromium powder, metal vanadium powder and pore-forming agent into a ball mill tank and mixing powder to obtain mixed powder, the mass percentage of metal powder in the mixed powder is about 70% to 50%, making The mass percentage of the porogen is about 30% to 50%;
[0017] b. Cold press molding, put the mixed powder obtained in the previous step into the abrasive tool, perform cold press molding under a unidirectional pressure of 100-150MPa, and obtain a compact after ejecting the mold;
[0018] c. Vacuum sintering, put the above-mentioned compact into the charging tank, cover the lid, and vacuumize to make the vacuum reach 10 -3 After Pa, start sintering, the sintering temperature is 900-1200°C, the holding time is 1-3h, and finally the desired porous vanadium-chromium-titanium material is obtained.
[001...
Embodiment 1
[0024] The pore-forming agent ammonium bicarbonate is sieved to obtain a particle size of about 80-100 μm. The mass ratio of ammonium bicarbonate pore-forming agent to metal mixed powder is 3:1. After mixing evenly, add it to a stainless steel abrasive tool, and use a one-way hydraulic universal testing machine to press and form it. The forming pressure is 80 MPa, and the pressure is maintained for 1 minute to obtain a green body. Place the green body in a vacuum of 10 -3 Sinter in a Pa vacuum sintering furnace, the sintering temperature is 900°C, the holding time is 2h, and the porous material is obtained by cooling with the furnace.
Embodiment 2
[0026] The pore-forming agent ammonium bicarbonate is sieved to obtain a particle size of about 80-100 μm. The mass ratio of ammonium bicarbonate pore-forming agent to metal mixed powder is 2:1. After mixing evenly, add it to the stainless steel grinding tool. Then add the mixed powder into a stainless steel abrasive tool, and use a one-way hydraulic universal testing machine to press and form the mold with a molding pressure of 100 MPa, and hold the pressure for 1 minute to obtain a green body. Place the green body in a vacuum of 10 -3 Sinter in a Pa vacuum sintering furnace, the sintering temperature is 1100°C, the holding time is 2h, and the porous material is obtained by cooling with the furnace.
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