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Production technology for co-producing potassium sulfate and tripolycyanamide and production equipment thereof

A technology for melamine and a production process, which is applied to the production process of potassium sulfate co-producing melamine and the field of production equipment, can solve the problems of high energy consumption, high cost, load reduction of potassium sulfate devices, etc., and achieves low energy consumption, convenient processing, The effect of reducing pollution levels

Inactive Publication Date: 2018-06-19
四川川化青上化工有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] In view of this, the application provides a production process for potassium sulfate co-production of melamine, which solves the problem of high energy consumption and high cost of ammonia and carbon dioxide produced in the production process of melamine in the existing production process through water washing, while potassium sulfate production During the process, the by-produced hydrochloric acid expands the library and the potassium sulfate unit is forced to reduce the load

Method used

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  • Production technology for co-producing potassium sulfate and tripolycyanamide and production equipment thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0021] 1) the concentrated sulfuric acid, potassium chloride are input in the reaction furnace and react;

[0022] 2) the HCL produced in step 1) is delivered to the HCL condenser, then passed into the sulfuric acid washing tower for washing, and the resulting product is finally passed into the hydrochloric acid absorption tower to obtain hydrochloric acid;

[0023] 3) Pass urea into the reactor, then filter the obtained product with hot gas, recrystallize, and finally pass the obtained crystals into the trap, and the obtained products include melamine, ammonia and carbon dioxide;

[0024] 4) Pass the ammonia and carbon dioxide obtained in step 3) into the melamine tail gas absorption tower, and simultaneously pass the hydrochloric acid prepared in step 2) into the melamine tail gas absorption tower;

[0025] 5) After the melamine tail gas absorption tower washes and absorbs the synthetic ammonia in the tail gas of melamine production, the ammonium chloride liquid produced ent...

Embodiment 2

[0028] After being washed and absorbed by the melamine tail gas absorption tower, the carbon dioxide gas that removes the synthetic ammonia is washed, compressed, pretreated, dried, liquefied, and purified to obtain a liquid food-grade carbon dioxide product.

[0029] After washing and absorbing the melamine tail gas absorption tower to remove the carbon dioxide gas from synthetic ammonia, it can be washed, compressed, pretreated, dried, liquefied, and purified to obtain liquid food-grade carbon dioxide products. Such tail gas treatment reduces the degree of pollution to the environment. The effect of environmental protection, and low energy consumption, reduces production costs and improves profit margins.

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Abstract

The invention discloses a production technology for co-producing potassium sulfate and tripolycyanamide. The production technology comprises the following steps: sending a byproduct hydrochloric acidproduced during production of potassium sulfate to a tripolycyanamide tail gas absorbing tower, washing and absorbing synthetic ammonia in tail gas discharged during production of the tripolycyanamide, enabling produced ammonium chloride liquid to enter a heating concentrating tank, heating for concentrating by using steam, then entering a crystallizing separator, then cooling for crystallizing, and then entering a centrifugal dryer to obtain a finished ammonium chloride product. In such a synthesis process, ammonia and carbon dioxide tail gas produced during the production of the tripolycyanamide are well treated, and the byproduct hydrochloric acid produced during the production of the potassium sulfate is not required to be stored and transported to other regions for achieving application thereof, so that the situation that a potassium sulfate producing device is forced to reduce the load due to overstock of the hydrochloric acid is avoided, the economic loss is reduced, the production process is environmentally friendly and does not cause harm to production personnel and the environment, and the economic benefit is remarkable.

Description

technical field [0001] The invention relates to the technical field of chemical production technology, in particular to a production technology and production equipment for potassium sulfate co-production of melamine. Background technique [0002] Potassium sulfate is a salt composed of sulfate ions and potassium ions, usually in the form of colorless or white crystals, granules or powder, odorless, bitter, hard, chemically inactive, stable in the air, and the aqueous solution is neutral Potassium sulfate, insoluble in ethanol, is a high-efficiency chlorine-free potassium fertilizer, which has obvious yield-increasing effects on various crops, and is mainly used for the planting and compounding of chlorine-avoiding crops, such as tobacco, citrus, watermelon, tea and other economic crops Fertilizer raw materials can not only increase the yield of crops, but also improve the quality of crops. [0003] Melamine is a triazine nitrogen-containing heterocyclic organic compound us...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01D5/02C01C1/16C01B32/50C01B7/03
CPCC01D5/02C01B7/035C01C1/164
Inventor 肖斌雍毅孔梅钟长志
Owner 四川川化青上化工有限公司
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