Preparation method of bactericidal polyester fibers
A technology of polyester fiber and bactericide, which is applied in the field of preparation of bactericidal polyester fiber, can solve the problems of easy drop, insufficient bactericidal effect, uneven distribution of silver in silver fiber, etc., achieve strong bactericidal ability, improve bactericidal efficiency, and particle size small effect
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Embodiment 1
[0024] 1) After the 0.2mol / L silver nitrate solution is activated, add concentrated ammonia and hydrogen peroxide, and shake the reaction in a constant temperature shaking box at 45°C. The metal precipitates are filtered and dried in an oven at 100°C for 4 hours;
[0025] 2) Mix the silver powder prepared in step 1) with the dispersant, the bactericide composed of alkyl quaternary phosphonium salt and quaternary ammonium salt, and activated carbon to make a sterilization mixture. The weight percentage of each component of the sterilization mixture is: silver powder 2%, dispersion 1% of bactericide, 1% of bactericide, 1% of activated carbon;
[0026] 3) After the sterilization mixture and the polyester fiber raw material are melted and blended at high temperature, they are processed by a screw extruder to obtain a spinning melt;
[0027] 4) The spinning melt obtained in step 3) is subjected to injection drawing processing by an injection molding machine, heat-setting and drying are pe...
Embodiment 2
[0030] 1) After the activation treatment of 0.3mol / L silver nitrate solution, add concentrated ammonia and hydrogen peroxide, and oscillate the reaction in a constant temperature shaking box at 45°C. The metal precipitates generated are filtered and dried in an oven at 100°C for 4 hours;
[0031] 2) Mix the silver powder prepared in step 1) with the dispersant, the bactericide composed of alkyl quaternary phosphonium salt and quaternary ammonium salt, and activated carbon to make a sterilization mixture. The weight percentage of each component of the sterilization mixture is: silver powder 4%, dispersion 2% of bactericide, 1% of bactericide, 1% of activated carbon;
[0032] 3) After the sterilization mixture and the polyester fiber raw material are melted and blended at high temperature, they are processed by a screw extruder to obtain a spinning melt;
[0033] 4) The spinning melt obtained in step 3) is subjected to injection drawing processing by an injection molding machine, heat-...
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