Dental repair filling material and preparation method thereof
A filling material and tooth technology, used in dental preparations, dentistry, dental prostheses, etc., can solve the problems of insufficient compressive strength and long coagulation time, and achieve the effects of simple method, short coagulation time and easy-to-obtain raw materials
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[0015] The present invention provides a kind of preparation method of filling material for tooth repair, and described preparation method comprises:
[0016] (1) After mixing tetracalcium phosphate, hydroxyapatite, calcium magnesium phosphate, anhydrous calcium hydrogen phosphate, anhydrous magnesium sulfate, sodium chloride and sodium bicarbonate, grind to obtain mixed powder M;
[0017] (2) mixing the mixed powder, solvent, adhesive, fibrous filler and biological filler to obtain a filling material for tooth restoration;
[0018] Wherein, relative to 100 parts by weight of tetracalcium phosphate, the consumption of hydroxyapatite is 40-60 parts by weight, the consumption of calcium magnesium phosphate is 20-40 parts by weight, and the consumption of anhydrous calcium hydrogen phosphate is 10-20 parts by weight, The consumption of anhydrous magnesium sulfate is 4-10 parts by weight, the consumption of sodium chloride is 1-10 parts by weight, and the consumption of sodium bica...
Embodiment 1
[0030] Tetracalcium phosphate, hydroxyapatite, magnesium calcium phosphate, anhydrous calcium hydrogen phosphate, anhydrous magnesium sulfate, sodium chloride and sodium bicarbonate are mixed and ground to obtain mixed powder M; mixed powder, ethanol, acrylate, Glass fiber and bioglass are mixed to obtain dental filling material A1;
[0031] Wherein, relative to the tetracalcium phosphate of 100g, the consumption of hydroxyapatite is 40g, the consumption of calcium magnesium phosphate is 20g, the consumption of anhydrous calcium hydrogen phosphate is 10g, the consumption of anhydrous magnesium sulfate is 4g, the consumption of sodium chloride For 1g, the consumption of sodium bicarbonate is 5g; Relative to the mixed powder of 100g, the consumption of ethanol is 70g, and the consumption of acrylate is 10g, and the consumption of glass fiber is 5g, and the consumption of bioglass is 5g.
Embodiment 2
[0033] Tetracalcium phosphate, hydroxyapatite, magnesium calcium phosphate, anhydrous calcium hydrogen phosphate, anhydrous magnesium sulfate, sodium chloride and sodium bicarbonate are mixed and ground to obtain mixed powder M; mixed powder, propylene glycol, methacrylic acid Salt, polyester fiber and calcium phosphate are mixed to obtain dental filling material A2;
[0034] Wherein, relative to the tetracalcium phosphate of 100g, the consumption of hydroxyapatite is 60g, the consumption of calcium magnesium phosphate is 40g, the consumption of anhydrous calcium hydrogen phosphate is 20g, the consumption of anhydrous magnesium sulfate is 10g, the consumption of sodium chloride For 10g, the consumption of sodium bicarbonate is 15g; Relative to the mixed powder of 100g, the consumption of propylene glycol is 100g, the consumption of methacrylate is 18g, the consumption of polyester fiber is 10g, and the consumption of calcium phosphate is 10g.
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