Superhydrophobic inorganic material powder and preparation method thereof
An inorganic material and super-hydrophobic technology, applied in the direction of inorganic pigment treatment, chemical instruments and methods, fibrous fillers, etc., to achieve the effect of rich raw material sources, good wear resistance and hydrophobicity, and low cost
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Embodiment 1
[0072] A commercially available industrial-grade silica hydrosol (purchased from Shandong Baxter New Material Co., Ltd.) with an average particle size of 15nm and a solid content of 20% is used as the raw material. The preparation process is as follows figure 1 As shown, achieved through the following steps:
[0073] 1. Adjust the silica nanoparticle hydrosol to a solid content of 40% through an ultrafiltration membrane system (purchased from Xiamen Kunyang Membrane Technology Co., Ltd.).
[0074] 2. Heat the concentrated silica nanoparticle hydrosol to 85°C and keep it for 24 hours to form a gel.
[0075] 3. Dry the gel in an oven at 200°C for 4 hours.
[0076] 4. Take 100g of the dried gel mass, grind it to a dry rubber powder dispersion with an average particle size of 500 microns, and then disperse it in 1L 95 volume industrial ethanol solution, add 0.5% ethanol volume while stirring Concentrated ammonia solution (concentration of 28% by volume) and trimethylmethoxysilane equivale...
Embodiment 2
[0080] It was prepared by the basic method as in Example 1, except that a commercially available industrial-grade silica hydrosol (purchased from Shandong Baxter New Materials Co., Ltd.) with an average particle size of 100 nm and a solid content of 20% was used as Raw material, the silica nano-particle hydrosol is adjusted to a solid content of 50% through an ultrafiltration membrane system.
Embodiment 3
[0082] A commercially available industrial-grade alumina hydrosol (purchased from Shandong Baxter New Material Co., Ltd.) with an average particle diameter of 100 nm and a solid content of about 20% is used as a raw material.
[0083] Prepared as figure 1 As shown, achieved through the following steps:
[0084] 1. Adjust the alumina nanoparticle hydrosol to a solid content of 50% through the ultrafiltration membrane system.
[0085] 2. Heat the concentrated alumina nanoparticle hydrosol to 85°C and keep it for 48 hours to form a gel.
[0086] 3. Dry the gel in an oven at 200°C for 4 hours.
[0087] 4. Take 100g of the dried gel mass, grind it to a dry rubber powder dispersion with an average particle size of 500 microns, and then disperse it in 1L 95 volume industrial ethanol solution, add 0.5% ethanol volume while stirring Concentrated ammonia solution (concentration of 28% by volume) and trimethylmethoxysilane equivalent to 3% of the weight of the gel mass are reacted at room tempera...
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