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A kind of steel pipe drawing emulsified oil with ultra-high lubricating performance and preparation method thereof

A technology of lubricating performance and emulsified oil, which is applied in the direction of lubricating composition, petroleum industry, etc., can solve the problems of surface finish, brightness reduction, adverse effects of heat treatment and annealing quality of drawn workpieces, welded pipes without matching lubricating oil, etc., to achieve Not easy to deteriorate, prevent sintering, and easy to operate

Active Publication Date: 2021-01-22
NANJING INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the steel pipe drawing lubricating oil has the problem of poor lubrication and cooling effect. After the steel pipe has been drawn many times, a large amount of metal powder is bonded to the surface of the drawn pipe and the edge of the hole core, resulting in a sharp increase in the friction coefficient between the two. Large, not only sharply reduce the surface finish and brightness of the drawn workpiece, but also aggravate the wear of the mold and affect the service life of the mold
In recent years, welded steel pipes have developed rapidly due to the advantages of simple production process, high production efficiency, low cost, high precision, uniform wall thickness, and arbitrary size. However, welded pipes do not have matching lubricating oil, and often Occurrence of quality problems of weld cracking due to local overheating of the steel pipe or mold
In addition, the currently used drawing lubricating oil is not easy to clean, which will have a negative impact on the heat treatment and annealing quality of the drawn steel pipe.

Method used

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  • A kind of steel pipe drawing emulsified oil with ultra-high lubricating performance and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] Embodiment 1 formula sees the following table:

[0017] serial number component name Weight (Kg) 1 Oil-soluble Nano-Fe 3 o 4 (2-50nm)

[0018] Production method: According to the weight formula of each component in the above table, first put 120kg of palm oil and 740kg of mechanical oil N68 into the reaction kettle with a rotation speed of 50-120 rpm for heating and stirring, when the temperature reaches 60-80°C, then sequentially 2kg oil-soluble nano-Fe 3 o 4 (2-50nm), 4kg nitrogen-containing borate, 2kg zinc dialkyl dithiophosphate, 30kg butyl stearate, 30kg C8-C10 mixed alcohol, 3kg sodium dodecylbenzenesulfonate and 3kg dimercaptothiol Add oxadiazole into the reaction kettle, keep warm and keep stirring for 60-100 minutes, then when the temperature drops to 70°C, add 20kg sorbitan oleate Span80, 20kg nonylphenol polyoxyethylene ether, 20kg triethanolamine, 3kg of methyl silicone oil and 3kg of pentachloronitrobenzene, adjust the speed of the...

Embodiment 2

[0020] Production method is with embodiment 1, and component name and percentage by weight thereof are shown in the following table:

[0021] serial number component name Weight percent (100%) 1 Oil-soluble Nano-Fe 3 o 4 (2-50nm)

[0022] Production method: According to the weight formula of each component in the above table, first put 150kg of palm oil and 390kg of mechanical oil N68 into the reaction kettle with a rotation speed of 50-120 rpm for heating and stirring, when the temperature reaches 60-80°C, then sequentially 10kg oil-soluble nano-Fe 3 o 4 (2-50nm), 20kg nitrogen-containing borate, 30kg zinc dialkyl dithiophosphate, 60kg butyl stearate, 80kg C8-C10 mixed alcohol, 20kg sodium dodecylbenzenesulfonate and 15kg dimercaptothiol Add oxadiazole into the reaction kettle, keep warm and keep stirring for 60-100 minutes, then when the temperature drops to 70°C, add 50kg sorbitan oleate Span80, 40kg nonylphenol polyoxyethylene ether, 80kg triethanol...

Embodiment 3

[0024] Embodiment 3 formula sees the following table:

[0025] serial number component name Weight percent (100%) 1 Oil-soluble Nano-Fe 3 o 4 (2-50nm)

15 2 nitrogen borate 30 3 Zinc Dialkyl Dithiophosphate 45 4 Butyl stearate 100 5 C8-C10 mixed alcohol 80 6 Sorbitan Oleate Span80 60 7 Nonylphenol polyoxyethylene ether 60 8 Triethanolamine 100 9 SDBS 30 10 Dimercaptothiadiazole 20 11 Pentachloronitrobenzene 30 12 Methicone 40 13 palm oil 180 14 Machine oil N68 210

[0026] Production method: According to the weight formula of each component in the above table, first put 180kg of palm oil and 210kg of mechanical oil N68 into the reaction kettle with a rotation speed of 50-120 rpm for heating and stirring, when the temperature reaches 60-80°C, then sequentially 15kg oil-soluble nano-Fe 3 o 4 (2-50nm), 30kg nitrogen-containing borate, 45kg zinc dialkyl dithioph...

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Abstract

The invention relates to a steel pipe drawing emulsified oil with ultrahigh lubricating property and a preparation method thereof. The method comprises the following steps: palm oil and machine oil N68 are first poured into a reaction kettle at the rotational speed of 50 to 120 rotations per minutes, heated and agitated; when temperature reaches 60 DEG C to 80 DEG C, oil-soluble nano Fe3O4 (2nm to50nm), nitrogen-containing borate, zinc dialkylphosphorodithiloate, butyl stearate, C8-C10 mixed alcohol, sodium dodecyl benzene sulfonate and dimercaptothiodiazole are then sequentially added into the reaction kettle, and agitation is continued for 60 to 100 minutes while temperature is kept; afterwards, when temperature is decreased to 70 DEG C, sorbitan monooleate Span 80, nonyl phenol polyoxyethylene ether, triethanolamine, methylsilicone oil and quintozene are added, the rotational speed of an agitator is adjusted to 30 rotations per minutes and agitation is kept for 30 to 60 minutes, heating is then stopped, agitation is continued until room temperature is reached, and thereby the welded pipe drawing emulsified oil which is yellowish-brown, transparent and uniform is obtained. The product disclosed by the invention is easy to degrade, the anticorrosive period is longer, the annealing detergency is better, and moreover, environment pollution can be reduced.

Description

technical field [0001] The invention relates to the technical field of lubricants, which are used for lubrication in the cold drawing process of various steel pipes such as stainless steel and high-temperature alloys, especially welded pipes. Specifically, it is a steel pipe drawing emulsified oil with ultra-high lubricating performance and its The preparation method is a steel pipe drawing emulsified oil that can prevent welding seam cracking and oxidative discoloration caused by local overheating of the surface of the welded pipe during cold drawing, and can ensure the surface brightness of the finished product. Background technique [0002] The drawing process is a typical plastic processing method. Under the action of drawing, the cross-sectional area of ​​the metal processing material is reduced through the core of the die to obtain a high-precision, high-gloss wire or pipe. During the drawing process, due to the large amount of metal deformation and the continuous gene...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10M169/04C10N30/06C10N40/24C10N50/00C10N30/12
CPCC10M169/048C10M2201/062C10M2203/1006C10M2207/021C10M2207/281C10M2207/289C10M2207/401C10M2209/104C10M2209/108C10M2215/042C10M2215/202C10M2219/044C10M2219/106C10M2223/045C10M2227/061C10M2229/041C10N2030/06C10N2030/12C10N2040/24C10N2030/56C10N2040/246C10N2050/01C10N2020/06C10N2020/093C10N2010/02C10N2010/04
Inventor 熊桑王章忠初雅杰王珏毛向阳
Owner NANJING INST OF TECH