Tooth repair filling material and preparation method thereof
A filling material and tooth technology, applied in dental preparations, dentistry, dental prostheses, etc., can solve the problems of insufficient compressive strength and long setting time, and achieve the effect of simple method, short setting time and high compressive strength
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[0015] The present invention provides a kind of preparation method of filling material for tooth repair, and described preparation method comprises:
[0016] (1) Calcium dihydrogen phosphate monohydrate, calcium dihydrogen phosphate anhydrous, calcium hydrogen phosphate dihydrate, calcium hydrogen phosphate anhydrous, magnesium sulfate anhydrous, sodium chloride and sodium bicarbonate are mixed and ground to obtain a mixed powder M;
[0017] (2) mixing the mixed powder, solvent, adhesive, fibrous filler and biological filler to obtain a filling material for tooth restoration;
[0018] Wherein, relative to 100 parts by weight of calcium dihydrogen phosphate monohydrate, the consumption of calcium dihydrogen phosphate anhydrous is 40-60 parts by weight, the consumption of calcium hydrogen phosphate dihydrate is 20-40 parts by weight, and the consumption of calcium hydrogen phosphate anhydrous is 20-40 parts by weight. The consumption is 10-20 parts by weight, the consumption of...
Embodiment 1
[0030] Calcium dihydrogen phosphate monohydrate, calcium dihydrogen phosphate anhydrous, calcium hydrogen phosphate dihydrate, calcium hydrogen phosphate anhydrous, magnesium sulfate anhydrous, sodium chloride and sodium bicarbonate are mixed and ground to obtain mixed powder M; Mixing powder, ethanol, acrylate, glass fiber and bioglass to obtain dental filling material A1;
[0031] Wherein, relative to 100g of calcium dihydrogen phosphate monohydrate, the consumption of calcium dihydrogen phosphate anhydrous is 40g, the consumption of calcium hydrogen phosphate dihydrate is 20g, the consumption of calcium hydrogen phosphate anhydrous is 10g, the consumption of anhydrous magnesium sulfate For 4g, the consumption of sodium chloride is 1g, and the consumption of sodium bicarbonate is 5g; Relative to the mixed powder of 100g, the consumption of ethanol is 70g, and the consumption of acrylate is 10g, and the consumption of glass fiber is 5g, and the consumption of bioglass The dos...
Embodiment 2
[0033] Calcium dihydrogen phosphate monohydrate, calcium dihydrogen phosphate anhydrous, calcium hydrogen phosphate dihydrate, calcium hydrogen phosphate anhydrous, magnesium sulfate anhydrous, sodium chloride and sodium bicarbonate are mixed and ground to obtain mixed powder M; The mixed powder, propylene glycol, methacrylate, polyester fiber and calcium phosphate are mixed to obtain the dental filling material A2;
[0034] Wherein, relative to 100g of calcium dihydrogen phosphate monohydrate, the consumption of calcium dihydrogen phosphate anhydrous is 60g, the consumption of calcium hydrogen phosphate dihydrate is 40g, the consumption of calcium hydrogen phosphate anhydrous is 20g, the consumption of anhydrous magnesium sulfate The amount of sodium chloride is 10g, the amount of sodium chloride is 10g, the amount of sodium bicarbonate is 15g; relative to 100g of mixed powder, the amount of propylene glycol is 100g, the amount of methacrylate is 18g, the amount of polyester f...
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