Nanometer composite material with high dielectric constant and low conductivity
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[0022] The present invention will be further elaborated below in conjunction with examples, but the present invention is not limited to specific embodiments.
[0023] 1) Using ultrasound-assisted Hummer’s method to prepare small graphene sheets, using 12000 mesh expanded graphite powder as the raw material.
[0024] 2) Take out the concentrated graphene flake solution obtained in (1) and dissolve it into DMF, add one of dihydroxydiphenyl ether, p-aminophenol, diaminodiphenyl sulfide, and diaminonaphthalene, and stir uniformly. The solution was centrifuged and washed three times with DMF solution to remove unreacted small organic molecules, then concentrated, collected and measured for concentration.
[0025] 3) Dissolve PVDF in DMF, mix it with the graphene material that adsorbs organic small molecules in (2) to form a graphene / PVDF solution, stir mechanically for 2 hours, ultrasonically disperse for 30 minutes, and put it in a vacuum oven for 2 hours to discharge the solution Disso...
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