Environment-friendly oxygen-resistant corrosion inhibitor for oilfield surface gathering pipelines and preparation method thereof
A technology for gathering and transportation pipelines and corrosion inhibitors, which is applied in the field of environment-friendly oxygen-resistant corrosion inhibitors for oil field surface gathering and transportation pipelines and its preparation, can solve the problems of unfavorable human beings and the environment, high toxicity, etc., and achieve the purpose of inhibiting metal corrosion and easily non-toxic effect
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[0031] The preparation method of described imidazole type quaternary ammonium salt, comprises the following steps:
[0032] (1) Add benzoic acid, xylene, and zinc particle catalyst to the reactor, stir evenly, slowly add diethylenetriamine dropwise, after the dropwise addition, slowly raise the temperature to 140°C, keep the temperature for 2 hours, and then raise the temperature to 180°C , heat preservation reaction for 6 hours, after the reaction is completed, the xylene is concentrated and dried under reduced pressure; the weight ratio of the benzoic acid, the xylene and the zinc particles is 1:8:0.002;
[0033](2) Add dimethyl carbonate to the product obtained in step (1), raise the temperature to 85°C, keep the temperature for 5 hours, then add 1,4-dibromobutane, keep the temperature for 5 hours, after the reaction, cool down to room temperature Add acetone, heat up to 60°C, keep warm for 1h, cool down to 0-5°C, keep warm for 1h, filter, and dry under reduced pressure to ...
Embodiment 1
[0048] The environment-friendly oxygen-resistant corrosion inhibitor for oilfield surface gathering and transportation pipelines, in parts by weight, at least includes 32 parts of corrosion inhibitor main agent, 7 parts of synergist, 1 part of surfactant, 45 parts of solvent, 13 parts of amino acid and 5 parts of amino acid Part oxygen scavenger; The main agent of the corrosion inhibitor includes 15 parts of imidazole type quaternary ammonium salts and 17 parts of Mannich bases in parts by weight; the synergist includes 3 parts of organic acetylenic alcohols and 4 parts plant extract; said amino acid is a mixture of cysteine, L-lysine and L-histidine, said cysteine, said L-lysine and said L-histidine The weight ratio of the acids is 1:0.6:0.3; the plant extract is a mixture of Fangji extract, banyan leaf extract, mugwort extract and lettuce extract, the Fangji extract, the banyan leaf extract, The weight ratio of the mugwort extract to the lettuce extract is 1:0.3:0.3:1.2; the...
Embodiment 2
[0057] The environment-friendly oxygen-resistant corrosion inhibitor for the oil field ground gathering and transportation pipeline, in parts by weight, at least includes 32 parts of corrosion inhibitor main agent, 7 parts of synergist, 1 part of surfactant, 45 parts of solvent, 13 parts of amino acid and 5 parts of oxygen scavenger; the main agent of the corrosion inhibitor includes 15 parts of imidazole type quaternary ammonium salt and 17 parts of Mannich base by weight; the synergist includes 3 parts of organic alkyne Alcohol and 4 parts of plant extracts; the amino acid is a mixture of cysteine, L-lysine and L-histidine, the cysteine, the L-lysine and the L- The weight ratio of histidine is 1:0.2:0.1; the plant extract is a mixture of Fangji extract, banyan leaf extract, mugwort extract and lettuce extract, the Fangji extract, the banyan leaf extract The weight ratio of the mugwort extract and the lettuce extract is 1:0.3:0.3:1.2; the raw materials for the preparation of ...
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