Preparation method of silicon dioxide hydrogel protein peptide mask
A technology of hydrogel protein and silicon dioxide, applied in cosmetic preparations, preparations for skin care, cosmetics, etc., can solve the problems of low content of nutrients in facial masks, poor skin surface cleaning effect, and poor preservation effect of nutrients, etc. To achieve the effect of hypoallergenic, promote blood circulation, simple operation and easy control
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Embodiment 1
[0021] A preparation method of silica hydrogel protein peptide facial mask, the specific steps of the preparation method are as follows:
[0022] (1) Isolate soybean protein peptide
[0023] Commercially available soybeans were used as raw materials, and the ratio of soybean mass to distilled water volume was 1kg:10L, and stirred and washed for 10min under the condition of 1000r / min. Then crush the washed soybeans, pass the crushed material through an 80-mesh sieve, and then add 0.15mol / L NaOH solution to the sieved material according to the ratio of mass to volume: 1kg:8L, stir well and allow it to fully react for 2 hours . Then put the above mixture into the reaction kettle, the reaction temperature is 800°C, the pressure is 8-10MPa, after the high temperature and high pressure treatment, the mixed solution is pumped into the horizontal screw centrifuge, and the centrifugation is carried out at the speed of 2000r / min. The centrifuged supernatant was acidified with 0.1 mol / ...
Embodiment 2
[0029] A preparation method of silica hydrogel protein peptide facial mask, same as embodiment 1, wherein:
[0030] 1) Isolate soybean protein peptide
[0031]Commercially available soybeans were used as raw materials, and the ratio of soybean mass to distilled water volume was 1 kg: 12.5 L, and stirred and washed for 10 min under the condition of 1500 r / min. Then crush the washed soybeans, pass the crushed material through a 80-mesh sieve, and then add 0.15mol / L NaOH solution to the sieved material according to the ratio of mass to volume: 1kg:9L, stir well and allow it to fully react for 2 hours . Then put the above mixture into the reaction kettle, the reaction temperature is 850°C, the pressure is 8MPa, after the high temperature and high pressure treatment, the mixed solution is pumped into the horizontal screw centrifuge, and the centrifugation is carried out under the condition of the rotating speed of 2000r / min, using 0.1 The mol / L phosphate buffer solution acidifies...
Embodiment 3
[0037] A preparation method of silica hydrogel protein peptide facial mask, same as embodiment 1, wherein:
[0038] Using commercially available soybeans as raw materials, according to the ratio of soybean mass to distilled water volume of 1kg:15L, stirring and washing were carried out at 1750r / min for 10min. Then crush the washed soybeans, pass the crushed material through a 80-mesh sieve, and then add 0.15mol / L NaOH solution to the sieved material according to the ratio of mass to volume: 1kg:9L, stir well and allow it to fully react for 2 hours . Then put the above mixture into the reaction kettle, the reaction temperature is 850°C, the pressure is 9MPa, after the high temperature and high pressure treatment, the mixed solution is pumped into the horizontal screw centrifuge, and the centrifugal separation is carried out under the condition of the rotating speed of 2500r / min, using 0.1 The mol / L phosphate buffer solution acidifies the centrifuged supernatant to make the pH=...
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