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Preparation method of high-toughness impact-resistant PET protective film

A technology of impact resistance and protective film, which is applied in the field of preparation of high-toughness and impact-resistant PET protective film, which can solve the problems of insufficient toughness of PET protective film, easy tearing of PET protective film, and poor impact resistance, so as to improve toughness And the effects of impact resistance, enhanced connection density, and enhanced dispersion

Inactive Publication Date: 2018-11-30
FOSHAN GAOMING DISTRICT ZHUAHE NEW MATERIAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The technical problem to be solved by the present invention is to provide a preparation method of a high-toughness and impact-resistant PET protective film in view of the defects that the current PET protective film has insufficient toughness and poor impact resistance, which cause the PET protective film to be easily torn and smashed

Method used

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  • Preparation method of high-toughness impact-resistant PET protective film

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Experimental program
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Effect test

example 1

[0026]In terms of parts by weight, weigh 1.5 parts of calcium hydroxide powder, 0.6 parts of sucrose and 110 parts of distilled water into a beaker under a vacuum environment, mix and stir with a stirrer at a speed of 600r / min for 30min, and pour 500mL of Inject carbon dioxide gas at a rate of 1 / min, filter to obtain the filter residue, put it in an oven and dry it for 3 hours at a temperature of 110°C to obtain the reaction product; in parts by weight, weigh 8 parts of the above reaction product and 20 parts of distilled water in In the three-necked flask, the temperature of the three-necked flask was raised to 85°C, stirred and mixed with a stirrer at a speed of 600r / min for 30min, and after stirring, 0.5 parts of distearoyloxyisopropyl aluminate, 0.3 parts of ten Octamine, continue to stir for 3 hours, after stirring, suction filter to obtain a filter cake, put the filter cake in an oven and dry at a temperature of 110°C, after drying, grind and pass through a 200-mesh sieve...

example 2

[0028] In terms of parts by weight, weigh 1.7 parts of calcium hydroxide powder, 0.8 parts of sucrose and 115 parts of distilled water into a beaker under a vacuum environment, mix and stir with a stirrer at a speed of 620r / min for 35min, and pour 550mL of Pass carbon dioxide gas at a rate of 1 / min, filter to obtain the filter residue, put it in an oven and dry it for 3.5 hours at a temperature of 115°C to obtain the reaction product; in parts by weight, weigh 9 parts of the above reaction product and 22 parts of distilled water In the three-necked flask, raise the temperature of the three-necked flask to 87°C, stir and mix with a stirrer at a speed of 620r / min for 35min, and add 0.7 parts of distearoyloxyisopropyl aluminate, 0.4 parts of Octadecylamine, continue to stir for 3.5 hours, after stirring, suction filter to obtain a filter cake, put the filter cake in an oven and dry at a temperature of 115°C, after drying, grind and pass through a 200-mesh sieve to obtain a modifie...

example 3

[0030] In terms of parts by weight, weigh 1.8 parts of calcium hydroxide powder, 1.0 parts of sucrose and 120 parts of distilled water into a beaker under a vacuum environment, mix and stir with a stirrer at a speed of 650r / min for 40min, and pour 600mL of Inject carbon dioxide gas at a rate of 1 / min, filter to obtain the filter residue, put it in an oven and dry it for 4 hours at a temperature of 120°C to obtain the reaction product; in parts by weight, weigh 10 parts of the above reaction product and 25 parts of distilled water in In the three-necked flask, raise the temperature of the three-necked flask to 90°C, stir and mix with a stirrer at a speed of 650r / min for 40min, after stirring, add 0.8 parts of distearoyloxyisopropyl aluminate, 0.5 parts of ten Octamine, continue to stir for 4 hours, after stirring, suction filter to obtain a filter cake, put the filter cake in an oven to dry at a temperature of 120°C, and after drying, grind and pass through a 200-mesh sieve to o...

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Abstract

The invention relates to a preparation method of a high-toughness impact-resistant PET protective film, and belongs to the technical field of protective film preparation of electronic products. According to the preparation method, calcium hydroxide is used as a raw material, sucrose is adopted as a crystal form guiding agent, and carbon dioxide is introduced so as to produce a nano calcium carbonate material; and the nano calcium carbonate is modified by using distearyloxy isopropyl aluminate and octadecylamine, toughening treatment is conducted on the polymer by selecting methyl methacrylate,butadiene and styrene ternary polymer and utilizing the rigidity of the nano calcium carbonate and large quantities of chemical bonds which are formed among molecules of the PET protective film underthe action of the aluminate coupling agent; the obtained copolymer has a core-shell structure, and the shell phase is composed of methyl methacrylate which has large hardness and can be miscible withmethyl methacrylate in the polymer; and therefore, the hardness and impact resistance of the PET protective film can be further enhanced, and the toughness and mechanical strength of the PET protective film can be enhanced remarkably, and the preparation method has a broad application prospect.

Description

technical field [0001] The invention relates to a preparation method of a high-toughness and impact-resistant PET protective film, belonging to the technical field of preparation of protective films for electronic products. Background technique [0002] At the beginning, PET materials were mainly used in industry. For example, the Coca-Cola plastic bottles we see today are made of PET. Mainly used for surface protection of mobile phones and other electronic products, glass surface protection and heat insulation, UV protection, etc. Because the PET material has the advantages of light weight, good transparency and gas barrier, non-toxic, tasteless, etc., it has achieved rapid development. Since the 1990s, the production and application of plastic packaging materials have sprung up like mushrooms, and with the maturity of touch technology, PET materials are naturally used on various LCD screens, which is today's PET protective film. [0003] With the rapid development of IT ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L67/02C08L33/12C08L69/00C08K9/04C08K9/10C08K3/26C08G63/183C08G63/86C08J5/18
CPCC08G63/183C08G63/866C08J5/18C08J2367/02C08J2433/12C08J2469/00C08K9/04C08K9/10C08K2003/265C08K2201/011
Inventor 裘友玖蒋梦成朱彩娣
Owner FOSHAN GAOMING DISTRICT ZHUAHE NEW MATERIAL TECH CO LTD
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