Polyurethane thermal insulation board for refrigeration storage and refrigeration box and preparation method thereof
A technology of polyurethane insulation board and refrigerator, which is applied in the field of cold chain technology industry, can solve problems such as non-compliance with environmental protection requirements, harmful gases, economic losses, etc., and achieve the effects of easy installation and maintenance, convenient installation and maintenance, and cost reduction
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[0033] Example 1
[0034] Preparation of reinforcing fiber: 30 parts by weight of aramid fiber with a fiber length of 0.5-6mm;
[0035] Preparation of filler: take 20 parts by weight of 140-200 mesh quartz sand, 5 parts by weight of 100-200 mesh red phosphorus, and 5 parts by weight of 200 mesh montmorillonite;
[0036] Preparation of rigid polyurethane foam: take 75 parts by weight of polyester polyol HF-8730 (Huafeng), 25 parts by weight of polyester polyol HF-86304 (Huafeng), and 4.5 parts by weight of dimethylcyclohexylamine, 0.5 parts by weight of stannous octoate, 9 parts by weight of HFC-365mfc, 8 parts by weight of pentane, 1.3 parts by weight of water, 15 parts by weight of triethyl phosphate, 5 parts by weight of trimethylol phosphine oxide, foam stabilizer B8481 (Degussa ) 2 parts by weight, 232 parts by weight of polyphenyl polymethylene polyisocyanate M50 (Basf);
[0037] The weight ratio of the reinforcing fiber, the filler and the polyurethane rigid foam foam is 30:30:...
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[0038] Example 2
[0039] Preparation of reinforcing fiber: take 5 parts by weight of carbon fiber with an average fiber length of 10mm and 5 parts by weight of glass fiber with an average fiber length of 5mm;
[0040] Preparation of filler: take 10 parts by weight of 180 mesh gypsum powder;
[0041] Preparation of rigid polyurethane foam: take 27 parts by weight of polyether polyol HP2502 (Hongbaoli), 73 parts by weight of polyester polyol HF-8730 (Huafeng), 2 parts by weight of dimethylcyclohexylamine, three parts 1.6 parts by weight of ethylene diamine, 0.4 parts by weight of potassium isooctanoate-dipropylene glycol solution, 8 parts by weight of pentane, 7 parts by weight of HFC-245fa, CO 2 5 parts by weight, 1.1 parts by weight of water, 25 parts by weight of tris(2-chloropropyl) phosphate, 1.7 parts by weight of foam stabilizer B8460 (Degussa), polyphenyl polymethylene polyisocyanate PM-400 (million Hua Chemical) 258 parts by weight;
[0042] The weight ratio of the reinforcin...
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[0043] Example 3
[0044] Preparation of reinforcing fiber: take 60 parts by weight of glass fiber with an average fiber length of 5mm;
[0045] Preparation of rigid polyurethane foam: 100 parts by weight of polyether polyol H4110 (Hongbaoli), 2 parts by weight of triethanolamine, 1,3,5-tris(dimethylaminopropyl) symmetric hexahydrotriazine 1 Parts by weight, 2 parts by weight of foaming agent water, 1.15 parts by weight of water, 30 parts by weight of diphenyl isooctyl phosphate, 1.8 parts by weight of foam stabilizer AK8830 (Meister), polyphenyl polymethylene polyisocyanate M20S (Basf) 221 parts by weight;
[0046] The reinforcing fiber and the polyurethane rigid foam foam are formulated into a mixture according to the proportion, and the weight ratio of the reinforcing fiber and the polyurethane rigid foam foam is 60:40. The mixture is poured on the polycarbonate film (thickness 0.5mm) of the surface layer material on the lower surface of the substrate, and the surface layer mate...
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