Natural rhizoma gastrodiae compound preservative solution as well as preparation method and application thereof
A composite fresh-keeping and Gastrodia elata technology, applied in the direction of application, food ingredients containing natural extracts, food ingredients as anti-microbial preservation, etc., can solve the problems of beautiful appearance, poor color and taste, poor nutrition and health value, and no natural Gastrodia elata compound fresh-keeping liquid and other problems, to achieve the effect of good color and taste, beautiful appearance, and satisfying fresh food consumption habits
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[0025] Such as figure 1 As shown, the preparation method of the natural Gastrodia elata composite fresh-keeping liquid that the embodiment of the present invention provides comprises the following steps:
[0026] S101: Prunella vulgaris powder according to the material: liquid = 1:6~16 respectively add 60% ethanol solution, room temperature, 600W~1000W, ultrasonic 5min~10min, reflux at 80°C for 2h, extract twice, collect and combine the extracts. Let it settle, filter, and centrifuge the filtrate at 4000r / min for 10min, collect the centrifugate, concentrate under reduced pressure to 1 / 5-1 / 6 of the original volume, recover ethanol, and freeze-dry to obtain Prunella vulgaris extract;
[0027] S102: Dandelion powder according to material: liquid = 1:6-16, add extraction solvent, the extraction solvent is a mixture of ethanol and ethyl acetate (ethanol: ethyl acetate = 1:5-1:5). Room temperature, 600W ~ 1000W, ultrasonic 5min ~ 10min, reflux extraction at 80°C for 2h, extract twi...
Embodiment 1
[0089](1) Preparation of Prunella vulgaris extract: Accurately weigh degreased Prunella vulgaris powder and put it into a flat-bottomed flask, add 60% ethanol solution respectively according to material: liquid=1:6~16, place the flat-bottomed flask in a numerically controlled ultrasonic cleaner 600-1000W, room temperature ultrasound for 5-10 minutes, then reflux extraction at 80°C for 2 hours, extraction twice, and combined extracts were collected. Set aside to settle, filter with four layers of gauze, centrifuge the filtrate at 4000r / min for 10 minutes, discard impurities, collect the centrifugate, and concentrate the collected extract in a rotary evaporator at 45r / min, 45°C, 0.09MPa , until the concentrated volume is 1 / 5-1 / 6 of the original volume, and the ethanol is recovered. The concentrated extract was transferred to a clean petri dish, placed in a refrigerator at -20°C, and frozen into a solid ice cube. Then put the frozen concentrated liquid extract into a vacuum free...
Embodiment 2
[0098] The preparation of natural extract and the preparation of preservative are the same as in Example 1.
[0099] Use the Gastrodia elata fresh-keeping liquid prepared by the method described in Example 1 to keep fresh, and the application method is as follows: put the drained gastrodia elata into a vacuum preservation bag, pour into the fresh above-mentioned fresh-keeping liquid of Gastrodia elata weight 2-4%, seal, and pack in vacuum Gastrodia elata is stored at 20°C, and the storage effect can be observed for 6 months.
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