Method for preparing polyetheretherketone-diatomaceous earth composite materials
A technology of polyether ether ketone and composite materials, which is applied in the field of preparation of polyether ether ketone-diatomite composite materials, can solve the problems of poor mechanical properties of the system, poor interface bonding, high melt viscosity, etc., and avoid structural The effects of sharp changes in elasticity and elasticity, enhanced interface bonding, and improved mechanical properties
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example 1
[0023] In parts by weight, put 20 parts of low-melting alloy powder, 20 parts of whiskers, 8 parts of starch, 3 parts of glycerin, and 30 parts of water into a ball mill for mixing and ball milling, and pass through a 100-mesh sieve to obtain a mixed homogenate; Put soil and acid in a single-necked flask at a mass ratio of 1:30, stir and mix for 60 minutes at a speed of 500r / min to obtain a mixed slurry, then filter the mixed slurry to obtain a filter residue, and then wash the filter residue with deionized water 8 times, then the filter residue after washing was placed in an oven, and dried to constant weight at a temperature of 110°C to obtain the primary treatment diatomite; Put the mass ratio of 1:30 in a three-necked flask, and mix and stir for 60 minutes under the condition of the rotating speed of 500r / min to obtain the mixed material liquid, then filter the mixed material liquid to obtain a filter cake, then put the filter cake in an oven, Dry to constant weight at a t...
example 2
[0025]In parts by weight, 20 parts of whiskers, 8 parts of starch, 3 parts of glycerin, and 30 parts of water are mixed and ball milled in a ball mill, and passed through a 100-mesh sieve to obtain a mixed homogenate; : 30 is placed in a single-necked flask, and under the condition of 500r / min, the rotating speed is 500r / min, stirring and mixing for 60min to obtain a mixed slurry, and then the mixed slurry is filtered to obtain a filter residue, and then the filter residue is washed 8 times with deionized water, and then the washed residue The filter residue was placed in an oven and dried to constant weight at a temperature of 110°C to obtain a primary treatment diatomite; the primary treatment diatomite and a mass concentration of 2.6mg / mL dopamine solution were placed in a mass ratio of 1:30 In a three-neck flask, under the condition of a rotating speed of 500r / min, mix and stir for 60min to obtain a mixed material liquid, then filter the mixed material liquid to obtain a fi...
example 3
[0027] In parts by weight, 20 parts of low-melting alloy powder, 8 parts of starch, 3 parts of glycerin, and 30 parts of water are placed in a ball mill and mixed for ball milling, and passed through a 100-mesh sieve to obtain a mixed homogenate; Put it in a single-necked flask with a ratio of 1:30, stir and mix for 60 minutes at a speed of 500r / min to obtain a mixed slurry, then filter the mixed slurry to obtain a filter residue, then wash the filter residue 8 times with deionized water, and then wash The final filter residue was placed in an oven, and dried to constant weight at a temperature of 110°C to obtain a primary treatment of diatomite; the primary treatment of diatomite and a mass concentration of 2.6mg / mL dopamine solution in a mass ratio of 1:30 Put it in a three-necked flask, and mix and stir for 60 minutes at a speed of 500r / min to obtain a mixed material liquid, then filter the mixed material liquid to obtain a filter cake, and then put the filter cake in an ove...
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