A method for preparing a wear-resistant layer on a magnesium-based surface of a graphene oxide alloy by laser cladding
A laser cladding and wear-resistant layer technology, applied in metal material coating process, coating and other directions, can solve the problems of lack of preparation technology of graphene oxide-plated wear-resistant layer, high powder waste, long production cycle, etc. The effect of reducing delamination, improving surface hardness, and low risk factor
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Embodiment 1
[0028] Graphene oxide was ultrasonically pre-dispersed in analytical pure ethanol for 1 h, the temperature was at room temperature, and no water vapor was controlled throughout the process. The volume ratio was strictly controlled at 0.2:50, and then the resulting dispersion was poured into a precursor solution consisting of glycerol and tetraisopropyl titanate, sealed and sonicated for 1 hour. Among them, the volume ratio of glycerol and tetraisopropyl titanate is 10:0.4. Carry out hydrothermal treatment afterwards, wherein the volume of suspension liquid accounts for 50% of reactor volume. Then put it into the reaction furnace to heat, raise the temperature to 90°C at 5°C / min, keep it for 2h, then raise the temperature to 180°C at 3°C / min, and keep it for 10h. Cool in air after taking out the reactor. The resulting solution was taken out, centrifuged, and centrifuged several times by pouring analytical pure ethanol until the solution was colorless. The whole process is se...
Embodiment 2
[0031]Graphene oxide was ultrasonically pre-dispersed in analytical pure ethanol for 3 hours, the temperature was at room temperature, and no water vapor was controlled throughout. The volume ratio was strictly controlled at 0.2:50, and then the resulting dispersion was poured into a precursor solution consisting of glycerol and tetraisopropyl titanate, sealed and sonicated for 1 hour. Among them, the volume ratio of glycerol and tetraisopropyl titanate is 10:0.8. Carry out hydrothermal treatment afterwards, wherein the volume of suspension liquid accounts for 50% of reactor volume. Then put it into the reaction furnace to heat, raise the temperature to 90°C at 3°C / min, keep it for 1h, then raise the temperature to 180°C at 2°C / min, and keep it for 12h. Cool in air after taking out the reactor. The resulting solution was taken out, centrifuged, and centrifuged several times by pouring analytical pure ethanol until the solution was colorless. The whole process is sealed to e...
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