Method for producing ethanol by reusing anaerobic digestion effluent and refining tower residue
An anaerobic digestion and residual liquid technology, applied in the direction of fermentation, can solve the problems of poisoning ethanol fermentation yeast, reducing the utilization rate of raw materials, and reducing the utilization rate of raw materials, so as to avoid acid production in ethanol fermentation, improve the performance of ethanol fermentation, and utilize raw materials. rate increase effect
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Embodiment 1
[0062] The method for producing ethanol by reusing the anaerobic digestion effluent and the residual liquid of the refined tower of the present invention adopts the following process steps:
[0063] Mix the membrane filtrate and the refined tower residue in a ratio of 85:15, the volatile acid concentration is 600mg / L; take 100Kg of crushed corn flour, add 310L of mixed solution ingredients, and add high temperature resistant α-amylase (10U / g starch ), stir well and heat to 86°C and maintain for 200min; reduce the temperature to 60°C, add glucoamylase (180U / g starch), stir well and keep saccharification for 15min. After saccharification, the temperature is lowered to 30°C, and 15% (v / v) yeast seed liquid is added to start fermentation. After the fermentation is completed, ethanol, distillation waste liquid and refined tower liquid are obtained by distillation. The distillation waste was filtered with a 60-mesh filter cloth to obtain wet vinasse and vinasse clear liquid, which was...
Embodiment 2
[0066] The method for producing ethanol by reusing the anaerobic digestion effluent and the residual liquid of the refined tower of the present invention adopts the following process steps:
[0067] Mix the membrane filtrate and the refined tower residue in a ratio of 90:10, the volatile acid concentration is 400mg / L; take 100Kg of crushed brown rice powder, add 260L of mixed liquid ingredients, and add high-temperature resistant α-amylase (8U / g starch ), stir well and heat to 90°C and maintain for 100min; reduce the temperature to 58°C, add glucoamylase (150U / g starch), stir well and keep saccharification for 30min. After saccharification, the temperature is lowered to 30°C, and 10% (v / v) yeast seed liquid is inserted to start fermentation. After the fermentation is completed, ethanol, distillation waste liquid and refined tower liquid are obtained by distillation. The distillation waste was filtered with a 60-mesh filter cloth to obtain wet vinasse and vinasse clear liquid, wh...
Embodiment 3
[0070] The method for producing ethanol by reusing the anaerobic digestion effluent and the residual liquid of the refined tower of the present invention adopts the following process steps:
[0071] Mix the membrane filtrate and the refined tower residue in a ratio of 99:1, the volatile acid concentration is 100mg / L; take 1000Kg of crushed brown rice powder and add 2600L of mixed solution ingredients, add high temperature resistant α-amylase (15U / g starch) , After stirring, heat to 95°C and maintain for 100min; lower the temperature to 60°C, add glucoamylase (160U / g starch), stir well and keep for 30min saccharification. After saccharification, the temperature is lowered to 30°C, and 12% (v / v) yeast seed liquid is inserted to start fermentation. After the fermentation is completed, ethanol, distillation waste liquid and refined tower liquid are obtained by distillation. The distillation waste was filtered with a 60-mesh filter cloth to obtain wet vinasse and vinasse clear liquid...
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