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Coffee roasting cigarette pop beads for reducing free radical content of smoke and preparation method thereof

A free radical, coffee technology, applied in the application, tobacco, e-liquid filter and other directions, can solve the problems of not prominent roasting aroma, increase the irritation and miscellaneous gas of cigarettes, etc., to improve the roasting aroma and smoking taste. , Improve the quality of roasting aroma, the effect of simple operation

Inactive Publication Date: 2019-01-25
CHINA TOBACCO YUNNAN IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the roasted fragrance of the above-mentioned products obtained is not outstanding, and still contains a certain amount of macromolecular substances such as protein, pectin, and polysaccharides, which will be cracked to produce some harmful components during the smoking process of cigarettes, which will increase the quality of cigarettes. Suction irritation and fumes

Method used

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  • Coffee roasting cigarette pop beads for reducing free radical content of smoke and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] The preparation method of the popping beads for roasted coffee cigarettes with reduced smoke free radical content of the present embodiment is carried out as follows:

[0025] Weigh 10 parts of Vietnamese medium-grain coffee, 1 part of Greek large-grain coffee, and 5 parts of Brazilian coffee coffee powder into a round-bottomed flask for mixing, then add 100 parts of ethylene glycol and 0.01 part of dextrin-polysaccharide-iron complex, stir, and connect the flask mouth Condensate the tube, put it into an oil bath and heat it to 150°C, and reflux for 3 hours.

[0026] Add 200 parts of petroleum ether to the above reaction product, ultrasonically extract for 60 minutes, then shake and extract for 60 minutes, then carry out centrifugation for 15 minutes, take the upper layer liquid and filter it with an organic filter membrane, carry out vacuum distillation, remove the solvent, and obtain roasted coffee Aroma.

[0027] Dissolve 5 parts of the above roasted coffee aroma su...

Embodiment 2

[0032] The preparation method of the popping beads for roasted coffee cigarettes with reduced smoke free radical content of the present embodiment is carried out as follows:

[0033] Weigh 30 parts of Hainan medium coffee, 30 parts of Vietnamese medium coffee, 2 parts of Greek coffee and 3 parts of Taiwan coffee, 25 parts of Jamaican coffee and Yunnan coffee, and mix them in a round bottom flask, then add 250 parts of propylene glycol and 1 part of iron dextran complex, stir, connect the mouth of the flask with a condenser, then put it into an oil bath and heat to 250°C, condense and reflux for 0.5h.

[0034] Add 2000 parts of n-hexane and chloroform to the above reaction product, wherein, n-hexane and chloroform are mixed at a volume ratio of 1:1, ultrasonically extracted for 10 minutes, then shaken and extracted for 10 minutes, centrifuged for 4 minutes, and the upper liquid is filtered with an organic filter membrane Afterwards, vacuum distillation is carried out to remove ...

Embodiment 3

[0040] The preparation method of the popping beads for roasted coffee cigarettes with reduced smoke free radical content of the present embodiment is carried out as follows:

[0041] Weigh 30 parts of Indian medium coffee and Hainan medium coffee, 2 parts of Taiwan large coffee, and 18 parts of Yunnan small coffee powder into a round bottom flask, then add 200 parts of glycerin, 0.1 part of iron dextran compound, and stir. Connect the mouth of the flask with a condenser, put it into an oil bath and heat it to 200°C, and condense and reflux for 1 hour.

[0042] Add 1,000 parts of ethyl acetate to the above reaction product, ultrasonically extract for 30 minutes, then shake and extract for 30 minutes, then centrifuge for 4 minutes, take the upper liquid and filter it with an organic filter membrane, then carry out vacuum distillation to remove the solvent, and obtain coffee roasted Roasted aroma substance.

[0043] The above 10 parts of roasted coffee aroma substances were diss...

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Abstract

The invention relates to a coffee roasting cigarette pop bead for reducing the free radical content of smoke and a preparation method thereof. The method is performed as follows: coffee roasting aromasubstance is dissolved in water or glyceryl octyl decanoate to prepare a solution of 5 to 15 percents by mass, and then baicalin with 0.5 to 1 percents by mass of coffee roasting aroma substance is added, stirring at room temperature for 20 to 30 minutes, and placed in shade and shade to be alcoholized for 24 to 48 hours. The invention can remove smoke irritation or impurity gas substance such asmacromolecular substance to obtain pure flue-cured aroma substance, which can be added to cigarette pop beads to greatly improve the aroma and taste of rich cigarettes. The coffee roasting aroma compound of the invention and baicalin can be used in cigarette pop beads together, the free radical content in cigarette smoke can be remarkably reduced, the roasting aroma of cigarette and the taste ofcigarette smoking can be improved, the roasting aroma quality of cigarette products can be effectively improved, the amount of impurity gas can be reduced, and the comfort and coordination of cigarette can be improved.

Description

technical field [0001] The invention relates to a popping bead for cigarettes and a preparation method thereof, in particular to a method for preparing a popping bead for coffee roasting cigarettes which reduces the content of smoke free radicals, and belongs to the field of cigarette accessories. Background technique [0002] Popping bead cigarettes are pre-embedded with one or more flavor capsules in the filter tip, and the smoker can selectively pinch and pop the capsules to release the flavor during the smoking process. Explosive beads are a new technical way to add flavor, flavor and moisture to cigarettes, an effective support for "perceivable" in the category construction work, and a means to realize the rejuvenation and personalization of cigarette brands. [0003] However, even with the addition of cigarette popping beads, domestic cigarette products have certain deficiencies in terms of smoking quality and sensory comfort, such as weak aroma, strong dryness, insuff...

Claims

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Application Information

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IPC IPC(8): A24D3/06
CPCA24D3/061
Inventor 魏玉玲张承明王晋张涛陈建华耿永勤李晶田丽梅蒋次清王小龙李雪梅
Owner CHINA TOBACCO YUNNAN IND